ethyl 2-(2,4-dinitrophenylthio)-4-amino-6-(3-nitrophenyl)pyrimidine-5-carboxylate

Base Information

Chemical Name:ethyl 2-(2,4-dinitrophenylthio)-4-amino-6-(3-nitrophenyl)pyrimidine-5-carboxylate
CAS No.:1628799-83-6
Molecular Formula:C₁₉H₁₄N₆O₈S
Molecular Weight:486.422
Hs Code.:

Synonyms:ethyl 2-(2,4-dinitrophenylthio)-4-amino-6-(3-nitrophenyl)pyrimidine-5-carboxylate

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Chemical Property of ethyl 2-(2,4-dinitrophenylthio)-4-amino-6-(3-nitrophenyl)pyrimidine-5-carboxylate

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Technology Process of ethyl 2-(2,4-dinitrophenylthio)-4-amino-6-(3-nitrophenyl)pyrimidine-5-carboxylate

There total 4 articles about ethyl 2-(2,4-dinitrophenylthio)-4-amino-6-(3-nitrophenyl)pyrimidine-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1628799-75-6
ethyl 4-amino-2-mercapto-6-(3-nitrophenyl)pyrimidine-5-carboxylate

: 97-00-7
1-chloro-2,4-dinitro-benzene

: 1628799-83-6
ethyl 2-(2,4-dinitrophenylthio)-4-amino-6-(3-nitrophenyl)pyrimidine-5-carboxylate

Guidance literature:: With sodium hydroxide; In ethanol; for 3h; Reflux;
DOI:10.2174/1570180811666140401182419

Reference yield:

: 1628799-68-7
C₁₃H₁₄N₄O₄S

: 1628799-83-6
ethyl 2-(2,4-dinitrophenylthio)-4-amino-6-(3-nitrophenyl)pyrimidine-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: selenium(IV) oxide; acetic acid / 0.5 h / 20 °C

2: sodium hydroxide / ethanol / 3 h / Reflux

With selenium(IV) oxide; acetic acid; sodium hydroxide; In ethanol;
DOI:10.2174/1570180811666140401182419

Reference yield:

: 99-61-6
3-nitro-benzaldehyde

: 1628799-83-6
ethyl 2-(2,4-dinitrophenylthio)-4-amino-6-(3-nitrophenyl)pyrimidine-5-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 3 h / Reflux

2: selenium(IV) oxide; acetic acid / 0.5 h / 20 °C

3: sodium hydroxide / ethanol / 3 h / Reflux

With selenium(IV) oxide; acetic acid; sodium hydroxide; In ethanol;
DOI:10.2174/1570180811666140401182419