1,6-anhydro-2-azido-4-O-<(2-azido-2-deoxy-β-D-mannopyranosyl)uronic acid>-3-O-benzyl-2-deoxy-β-D-glucopyranose

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Chemical Name:1,6-anhydro-2-azido-4-O-<(2-azido-2-deoxy-β-D-mannopyranosyl)uronic acid>-3-O-benzyl-2-deoxy-β-D-glucopyranose
CAS No.:95451-86-8
Molecular Formula:C₁₉H₂₂N₆O₉
Molecular Weight:478.418
Hs Code.:

Synonyms:1,6-anhydro-2-azido-4-O-<(2-azido-2-deoxy-β-D-mannopyranosyl)uronic acid>-3-O-benzyl-2-deoxy-β-D-glucopyranose

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Chemical Property of 1,6-anhydro-2-azido-4-O-<(2-azido-2-deoxy-β-D-mannopyranosyl)uronic acid>-3-O-benzyl-2-deoxy-β-D-glucopyranose

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Technology Process of 1,6-anhydro-2-azido-4-O-<(2-azido-2-deoxy-β-D-mannopyranosyl)uronic acid>-3-O-benzyl-2-deoxy-β-D-glucopyranose

There total 7 articles about 1,6-anhydro-2-azido-4-O-<(2-azido-2-deoxy-β-D-mannopyranosyl)uronic acid>-3-O-benzyl-2-deoxy-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 95451-83-5
1,6-Anhydro-2-azido-4-O-(2-azido-2-desoxy-β-D-mannopyranosyl)-3-O-benzyl-2-desoxy-β-D-glucopyranose

: 95451-86-8
1,6-anhydro-2-azido-4-O-<(2-azido-2-deoxy-β-D-mannopyranosyl)uronic acid>-3-O-benzyl-2-deoxy-β-D-glucopyranose

Guidance literature:: With oxygen; platinum(IV) oxide; In propan-1-ol; water; at 80 ℃; for 6h; NaHCO₃, pH 7.5;
DOI:10.1016/0008-6215(86)80006-4

Reference yield:

: 55682-57-0
1,6-anhydro-2-azido-3-O-benzyl-2-deoxy-β-D-glucopyranose

: 95451-86-8
1,6-anhydro-2-azido-4-O-<(2-azido-2-deoxy-β-D-mannopyranosyl)uronic acid>-3-O-benzyl-2-deoxy-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: Silbersilicat / toluene

2: deacetylation

3: 82 percent / oxygen, sodium hydrogen carbonate / Adam's catalyst / H₂O

With Silbersilicat; oxygen; sodium hydrogencarbonate; platinum(IV) oxide; In water; toluene;
DOI:10.1016/0008-6215(84)85195-2

Reference yield:

: 95451-93-7
3,4,6-Tri-O-acetyl-2-azido-2-deoxy-α-D-mannopyranosyl bromide

: 95451-86-8
1,6-anhydro-2-azido-4-O-<(2-azido-2-deoxy-β-D-mannopyranosyl)uronic acid>-3-O-benzyl-2-deoxy-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: Silbersilicat / toluene

2: deacetylation

3: 82 percent / oxygen, sodium hydrogen carbonate / Adam's catalyst / H₂O

With Silbersilicat; oxygen; sodium hydrogencarbonate; platinum(IV) oxide; In water; toluene;
DOI:10.1016/0008-6215(84)85195-2