3-[1-(2-nitrobenzenesulfonyl)-5,10,14-tris-Boc-spermine]propanyl iodide

Base Information

• Chemical Name: 3-[1-(2-nitrobenzenesulfonyl)-5,10,14-tris-Boc-spermine]propanyl iodide
• CAS No.: 1131915-28-0
• Molecular Formula: C₃₄H₅₈IN₅O₁₀S
• Molecular Weight: 855.833

Synonyms:3-[1-(2-nitrobenzenesulfonyl)-5,10,14-tris-Boc-spermine]propanyl iodide

Chemical Property of 3-[1-(2-nitrobenzenesulfonyl)-5,10,14-tris-Boc-spermine]propanyl iodide

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Technology Process of 3-[1-(2-nitrobenzenesulfonyl)-5,10,14-tris-Boc-spermine]propanyl iodide

There total 1 articles about 3-[1-(2-nitrobenzenesulfonyl)-5,10,14-tris-Boc-spermine]propanyl iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C35H61N5O13S2 → 3-[1-(2-nitrobenzenesulfonyl)-5,10,14-tris-Boc-spermine]propanyl iodide (1131915-28-0)

Guidance literature:

With sodium iodide; In acetone; for 9h; Reflux; Inert atmosphere;

DOI:10.1021/jm801481y

Reference yield: 72.0%

Alloc-Lys(Ns)-OAll (1131915-43-9) + 3-[1-(2-nitrobenzenesulfonyl)-5,10,14-tris-Boc-spermine]propanyl iodide (1131915-28-0) → Nα-alloc-Nε-[3-[1-(2-nitrobenzenesulfonyl)-5,10,14-tris-Boc-spermine]propanyl]-Nε-(2-nitrobenzenesulfonyl)-L-lysine allyl ester (1131915-31-5)

Guidance literature:

With caesium carbonate; In acetonitrile; at 50 ℃; for 8h; Inert atmosphere;

DOI:10.1021/jm801481y

Reference yield: 64.0%

Dde-Lys(Ns)-OAll (1131915-46-2) + 3-[1-(2-nitrobenzenesulfonyl)-5,10,14-tris-Boc-spermine]propanyl iodide (1131915-28-0) → Nα-Dde-Nε-[3-[1-(2-nitrobenzenesulfonyl)-5,10,14-tris-Boc-spermine]propanyl]-Nε-(2-nitrobenzenesulfonyl)-L-lysine allyl ester (1131915-34-8)

Guidance literature:

With caesium carbonate; In acetonitrile; at 50 ℃; for 18h; Inert atmosphere;

DOI:10.1021/jm801481y

Downstream raw materials:

Nα-Dde-Nε-[3-[1-(2-nitrobenzenesulfonyl)-5,10,14-tris-Boc-spermine]propanyl]-Nε-(2-nitrobenzenesulfonyl)-L-lysine allyl ester

Nα-alloc-Nε-[3-[1-(2-nitrobenzenesulfonyl)-5,10,14-tris-Boc-spermine]propanyl]-Nε-(2-nitrobenzenesulfonyl)-L-lysine allyl ester

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