methoxy(5,10-diphenyl-15-(methyl pentanoate)subporphyrinato)boron(III)

Base Information

Chemical Name:methoxy(5,10-diphenyl-15-(methyl pentanoate)subporphyrinato)boron(III)
CAS No.:1392132-06-7
Molecular Formula:C₃₄H₃₀BN₃O₃
Molecular Weight:539.441
Hs Code.:

Synonyms:methoxy(5,10-diphenyl-15-(methyl pentanoate)subporphyrinato)boron(III)

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Chemical Property of methoxy(5,10-diphenyl-15-(methyl pentanoate)subporphyrinato)boron(III)

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Technology Process of methoxy(5,10-diphenyl-15-(methyl pentanoate)subporphyrinato)boron(III)

There total 8 articles about methoxy(5,10-diphenyl-15-(methyl pentanoate)subporphyrinato)boron(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: BnZnC₄H₈CO₂Me*LiCl

: 1392132-04-5
methoxo(5-bromo-10,15-diphenylsubporphyrinato)boron(III)

: 1392132-06-7
methoxy(5,10-diphenyl-15-(methyl pentanoate)subporphyrinato)boron(III)

Guidance literature:: With Pd-PEPPSI-IPent; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1002/anie.201201853

Reference yield: 50.0%

: 1392132-04-5
methoxo(5-bromo-10,15-diphenylsubporphyrinato)boron(III)

: 1392132-16-9
CH₃OC(O)CH₂CH₂CH₂CH₂^(1-)*Zn⁽²⁺⁾*Br^(1-)*Li⁽¹⁺⁾*Cl^(1-)=CH₃OC(O)C₄H₈ZnBr*LiCl

: 1392132-06-7
methoxy(5,10-diphenyl-15-(methyl pentanoate)subporphyrinato)boron(III)

Guidance literature:: dichloro(1,3-bis(2,6-bis(3-pentyl)phenyl)imidazolin-2-ylidene)(3-chloropyridyl)palladium(II); In tetrahydrofuran; room temp., 12 h;
DOI:10.1002/anie.201201853

Reference yield:

: 352423-56-4
C₂₂H₂₀N₂O

: 1392132-06-7
methoxy(5,10-diphenyl-15-(methyl pentanoate)subporphyrinato)boron(III)

Guidance literature:: Multi-step reaction with 5 steps

1.1: trifluoroacetic acid / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

2.1: 1,2-dichloro-benzene / 2 h / 150 °C / Inert atmosphere

3.1: 1,2-dichloro-benzene / 1 h / 100 °C

3.2: air / 1 h / Reflux

4.1: N-Bromosuccinimide / chloroform / 0.25 h / 0 °C

5.1: Pd-PEPPSI-IPent / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

With N-Bromosuccinimide; Pd-PEPPSI-IPent; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; chloroform; 1,2-dichloro-benzene; 5.1: Negishi coupling reaction;
DOI:10.1002/anie.201201853