(3Z,5E)-2,2,2-trichloro-N-(2,2-dimethyl-6-phenyl-3,5-hexadien-3-yl)acetamide

Base Information

• Chemical Name: (3Z,5E)-2,2,2-trichloro-N-(2,2-dimethyl-6-phenyl-3,5-hexadien-3-yl)acetamide
• CAS No.: 59403-07-5
• Molecular Formula: C₁₆H₁₈Cl₃NO
• Molecular Weight: 346.684

Synonyms:(3Z,5E)-2,2,2-trichloro-N-(2,2-dimethyl-6-phenyl-3,5-hexadien-3-yl)acetamide

Chemical Property of (3Z,5E)-2,2,2-trichloro-N-(2,2-dimethyl-6-phenyl-3,5-hexadien-3-yl)acetamide

Chemical Property:

Purity/Quality:

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Technology Process of (3Z,5E)-2,2,2-trichloro-N-(2,2-dimethyl-6-phenyl-3,5-hexadien-3-yl)acetamide

There total 3 articles about (3Z,5E)-2,2,2-trichloro-N-(2,2-dimethyl-6-phenyl-3,5-hexadien-3-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

2,2,2-Trichloro-acetimidic acid 1-benzyl-4,4-dimethyl-pent-2-ynyl ester (59402-99-2) → (3Z,5E)-2,2,2-trichloro-N-(2,2-dimethyl-6-phenyl-3,5-hexadien-3-yl)acetamide (59403-07-5)

Guidance literature:

In xylene; for 8h; Heating;

DOI:10.1021/ja00400a053

Reference yield:

5,5-dimethyl-1-phenyl-3-hexyn-2-ol (62969-96-4) → (3Z,5E)-2,2,2-trichloro-N-(2,2-dimethyl-6-phenyl-3,5-hexadien-3-yl)acetamide (59403-07-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / potassium hydride / tetrahydrofuran; hexane / 1.5 h / 0 °C

2: 68 percent / xylene / 8 h / Heating

With potassium hydride; In tetrahydrofuran; hexane; xylene;

DOI:10.1021/ja00400a053

Reference yield:

Potassium; 5,5-dimethyl-1-phenyl-hex-3-yn-2-olate → (3Z,5E)-2,2,2-trichloro-N-(2,2-dimethyl-6-phenyl-3,5-hexadien-3-yl)acetamide (59403-07-5)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

In diethyl ether;

DOI:10.1021/ja00424a068

upstream raw materials:

2,2,2-Trichloro-acetimidic acid 1-benzyl-4,4-dimethyl-pent-2-ynyl ester

5,5-dimethyl-1-phenyl-3-hexyn-2-ol

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