2,3-DICYANO-6-NITRONAPHTHALENE

Base Information

• Chemical Name: 2,3-DICYANO-6-NITRONAPHTHALENE
• CAS No.: 184026-06-0
• Molecular Formula: C12H5 N3 O2
• Molecular Weight: 223.19
• Hs Code.: 2926909090
• Mol file: 184026-06-0.mol

Synonyms:2,3-Dicyano-6-nitronaphthalene;6-Nitro-2,3-dicyanonaphthalene; 6-Nitro-2,3-naphthalonitrile

Chemical Property of 2,3-DICYANO-6-NITRONAPHTHALENE

Chemical Property:

• Melting Point: 250°C
• Boiling Point: 505.7±35.0 °C(Predicted)
• PSA: 93.40000
• Density: 1.43±0.1 g/cm3(Predicted)
• LogP: 3.01456
• Solubility.: slightly sol. in Toluene

Purity/Quality:

97% ^*data from raw suppliers

2,3-Dicyano-6-nitronaphthalene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,3-DICYANO-6-NITRONAPHTHALENE

There total 2 articles about 2,3-DICYANO-6-NITRONAPHTHALENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitro-o-xylene (99-51-4,34527-23-6,156617-88-8) → 6-nitronaphthalene-2,3-dicarbonitrile (184026-06-0)

Guidance literature:

Multi-step reaction with 2 steps

1: NBS, (PhCO)2O₂ / Irradiation

2: NaI

With N-Bromosuccinimide; sodium iodide; dibenzoyl peroxide;

Reference yield:

4-nitro-α,α,α',α'-tetrabromo-o-xylene (13209-16-0) + 1,2-Dicyanoethylene (764-42-1) → 6-nitronaphthalene-2,3-dicarbonitrile (184026-06-0)

Guidance literature:

With sodium iodide;

Reference yield: 42.0%

3,5-Di-tert-butylphenol (1138-52-9) + 6-nitronaphthalene-2,3-dicarbonitrile (184026-06-0) → 6-(3,5-Di-tert-butyl-phenoxy)-naphthalene-2,3-dicarbonitrile

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 50 - 70 ℃;

DOI:10.1002/(SICI)1521-3765(19980904)4:9<1633::AID-CHEM1633>3.0.CO;2-O

upstream raw materials:

4-nitro-α,α,α',α'-tetrabromo-o-xylene

1,2-Dicyanoethylene

4-nitro-o-xylene

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