Boc-Dab(Z)-Ser-OMe

Base Information

Chemical Name:Boc-Dab(Z)-Ser-OMe
CAS No.:84983-59-5
Molecular Formula:C₂₁H₃₁N₃O₈
Molecular Weight:453.492
Hs Code.:

Synonyms:Boc-Dab(Z)-Ser-OMe

Suppliers and Price of Boc-Dab(Z)-Ser-OMe

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Boc-Dab(Z)-Ser-OMe

Chemical Property:

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Technology Process of Boc-Dab(Z)-Ser-OMe

There total 1 articles about Boc-Dab(Z)-Ser-OMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 5680-80-8
methyl (2S)-2-amino-3-hydroxypropanoate hydrochloride

: 3350-20-7,47461-65-4,70882-68-7
(2S)-4-(benzyloxycarbonyl)amino-2-(tert-butoxycarbonyl)aminobutyric acid

: 84983-59-5
Boc-Dab(Z)-Ser-OMe

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1055/s-0029-1219155

Reference yield:

: 84983-59-5
Boc-Dab(Z)-Ser-OMe

: C₂₁H₂₉N₃O₇

Guidance literature:: With diethylamino-sulfur trifluoride; In dichloromethane; at -78 ℃; for 2h; Inert atmosphere;
DOI:10.1055/s-0029-1219155

Reference yield:

: 84983-59-5
Boc-Dab(Z)-Ser-OMe

: Z-Pyr-Ala-Dab(Z)-Ser-Gln-Gly-Gly-Ser-Asn-ONb

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) TFA, anisole 2.) HOBT, WSCl, NMM / 1.) room temperature, 20 min 2.) DMF, 4 deg C, overnight

2: 1.) TFA, anisole 2.) HOBT, WSCl, NMM / 1.) room temperature, 20 min 2.) DMF, 4 deg C, overnight

3: 94 percent / hydrazine hydrate / dimethylformamide; methanol / 48 h / Ambient temperature

With 4-methyl-morpholine; benzotriazol-1-ol; hydrazine hydrate; methoxybenzene; trifluoroacetic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.30.4448