5-[3-(Benzyl-methyl-amino)-4-(toluene-4-sulfonylamino)-phenoxy]-2-(toluene-4-sulfonylamino)-benzoic acid methyl ester

Base Information

Chemical Name:5-[3-(Benzyl-methyl-amino)-4-(toluene-4-sulfonylamino)-phenoxy]-2-(toluene-4-sulfonylamino)-benzoic acid methyl ester
CAS No.:951666-53-8
Molecular Formula:C₃₆H₃₅N₃O₇S₂
Molecular Weight:685.822
Hs Code.:

Synonyms:5-[3-(Benzyl-methyl-amino)-4-(toluene-4-sulfonylamino)-phenoxy]-2-(toluene-4-sulfonylamino)-benzoic acid methyl ester

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Chemical Property of 5-[3-(Benzyl-methyl-amino)-4-(toluene-4-sulfonylamino)-phenoxy]-2-(toluene-4-sulfonylamino)-benzoic acid methyl ester

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Technology Process of 5-[3-(Benzyl-methyl-amino)-4-(toluene-4-sulfonylamino)-phenoxy]-2-(toluene-4-sulfonylamino)-benzoic acid methyl ester

There total 2 articles about 5-[3-(Benzyl-methyl-amino)-4-(toluene-4-sulfonylamino)-phenoxy]-2-(toluene-4-sulfonylamino)-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: methyl 5-[4-amino-3-(benzyl-methyl-amino)-phenoxy]-2-(toluene-4-sulfonyl-amino)-benzoate

: 98-59-9
p-toluenesulfonyl chloride

: 951666-53-8
5-[3-(Benzyl-methyl-amino)-4-(toluene-4-sulfonylamino)-phenoxy]-2-(toluene-4-sulfonylamino)-benzoic acid methyl ester

Guidance literature:: methyl 5-[4-amino-3-(benzyl-methyl-amino)-phenoxy]-2-(toluene-4-sulfonyl-amino)-benzoate; p-toluenesulfonyl chloride; With pyridine; In dichloromethane; at 40 - 60 ℃;

With potassium hydrogensulfate; In dichloromethane; water;

Reference yield: 46.0%

: 951666-74-3
5-[4-Amino-3-(benzyl-methyl-amino)-phenoxy]-2-(toluene-4-sulfonyl-amino)-benzoic acid methyl ester

: 98-59-9
p-toluenesulfonyl chloride

: 951666-53-8
5-[3-(Benzyl-methyl-amino)-4-(toluene-4-sulfonylamino)-phenoxy]-2-(toluene-4-sulfonylamino)-benzoic acid methyl ester

Guidance literature:: 5-[4-Amino-3-(benzyl-methyl-amino)-phenoxy]-2-(toluene-4-sulfonyl-amino)-benzoic acid methyl ester; p-toluenesulfonyl chloride; With pyridine; In dichloromethane; for 24h; Reflux;

With potassium hydrogensulfate; In dichloromethane; water;

Reference yield: 68.0%

: 951666-53-8
5-[3-(Benzyl-methyl-amino)-4-(toluene-4-sulfonylamino)-phenoxy]-2-(toluene-4-sulfonylamino)-benzoic acid methyl ester

: 951666-77-6
methyl 5-[3-methylamino-4-(toluene-4-sulfonylamino)-phenoxy]-2-(toluene-4-sulfonylamino)-benzoate

Guidance literature:: 5-[3-(Benzyl-methyl-amino)-4-(toluene-4-sulfonylamino)-phenoxy]-2-(toluene-4-sulfonylamino)-benzoic acid methyl ester; With hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; acetic acid; at 50 ℃; for 6h; under 760.051 Torr;

With sodium hydrogencarbonate; In water; ethyl acetate;