Fe(N-benzyl-1-(pyridin-2-yl)-N-[(pyridin-2-yl)methyl]-methanamine)Cl₃

Base Information

• Chemical Name: Fe(N-benzyl-1-(pyridin-2-yl)-N-[(pyridin-2-yl)methyl]-methanamine)Cl₃
• CAS No.: 189687-38-5
• Molecular Formula: C₁₉H₁₉Cl₃FeN₃
• Molecular Weight: 451.586
• Mol file: 189687-38-5.mol

Synonyms:Fe(N-benzyl-1-(pyridin-2-yl)-N-[(pyridin-2-yl)methyl]-methanamine)Cl₃

Chemical Property of Fe(N-benzyl-1-(pyridin-2-yl)-N-[(pyridin-2-yl)methyl]-methanamine)Cl₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Fe(N-benzyl-1-(pyridin-2-yl)-N-[(pyridin-2-yl)methyl]-methanamine)Cl₃

There total 1 articles about Fe(N-benzyl-1-(pyridin-2-yl)-N-[(pyridin-2-yl)methyl]-methanamine)Cl₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

iron(III) chloride + N,N-di(2-picolyl)benzylamine (26082-96-2) → Fe(N-benzyl-1-(pyridin-2-yl)-N-[(pyridin-2-yl)methyl]-methanamine)Cl3 (189687-38-5)

Guidance literature:

In methanol; for 0.5h;

DOI:10.1016/j.poly.2014.02.018

Reference yield: 80.0%

3,5-Di-tert-butylcatechol (1020-31-1,122983-47-5,881376-69-8) + Fe(N-benzyl-1-(pyridin-2-yl)-N-[(pyridin-2-yl)methyl]-methanamine)Cl3 (189687-38-5) → [(C5H4NCH2)2N(C6H5CH2)]FeCl[[(CH3)3C]2C6H2(O2)] (325956-24-9)

Guidance literature:

With NaOCH₃; In dichloromethane; (N2); mixed, stirred (for 2 h); dried (in vac.), recrystd. (acetone); elem. anal.;

DOI:10.1002/1521-3773(20001201)39:23<4284::AID-ANIE4284>3.0.CO;2-I

Reference yield: 75.0%

Fe(N-benzyl-1-(pyridin-2-yl)-N-[(pyridin-2-yl)methyl]-methanamine)Cl3 (189687-38-5) + Benzohydroxamic acid (495-18-1) → [Fe(benzhydroxamate)(N-benzyl-1-(pyridin-2-yl)-N-[(pyridin-2-yl)methyl]-methanamine)Cl]Cl*H2O

Guidance literature:

With triethylamine; In methanol;

DOI:10.1016/j.poly.2014.02.018

upstream raw materials:

N,N-di(2-picolyl)benzylamine

Downstream raw materials:

[(C₅H₄NCH₂)2N(C₆H₅CH₂)]FeCl[[(CH₃)3C]2C₆H₂(O₂)]