(4S,5E,7E)-4-(benzyloxy)-N-hydroxy-11-(methoxymethoxy)undeca-5,7-dienamide

Base Information

Chemical Name:(4S,5E,7E)-4-(benzyloxy)-N-hydroxy-11-(methoxymethoxy)undeca-5,7-dienamide
CAS No.:622836-75-3
Molecular Formula:C₂₀H₂₉NO₅
Molecular Weight:363.454
Hs Code.:

Synonyms:(4S,5E,7E)-4-(benzyloxy)-N-hydroxy-11-(methoxymethoxy)undeca-5,7-dienamide

Suppliers and Price of (4S,5E,7E)-4-(benzyloxy)-N-hydroxy-11-(methoxymethoxy)undeca-5,7-dienamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S,5E,7E)-4-(benzyloxy)-N-hydroxy-11-(methoxymethoxy)undeca-5,7-dienamide

Chemical Property:

Purity/Quality:

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Technology Process of (4S,5E,7E)-4-(benzyloxy)-N-hydroxy-11-(methoxymethoxy)undeca-5,7-dienamide

There total 6 articles about (4S,5E,7E)-4-(benzyloxy)-N-hydroxy-11-(methoxymethoxy)undeca-5,7-dienamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 622836-81-1
(5E,7E)-(S)-4-Benzyloxy-11-methoxymethoxy-undeca-5,7-dienoic acid methyl ester

: 622836-75-3
(4S,5E,7E)-4-(benzyloxy)-N-hydroxy-11-(methoxymethoxy)undeca-5,7-dienamide

Guidance literature:: With potassium hydroxide; hydroxylamine hydrochloride; In methanol; at 0 ℃;
DOI:10.1021/ol030088w

Reference yield:

: (3S,6E)-3-(benzyloxy)-10-(methoxymethoxy)deca-4,6-dien-1-ol

: 622836-75-3
(4S,5E,7E)-4-(benzyloxy)-N-hydroxy-11-(methoxymethoxy)undeca-5,7-dienamide

Guidance literature:: Multi-step reaction with 6 steps

1: 91 percent / Et₃N; DMAP / CH₂Cl₂ / 20 °C

2: 94 percent / I₂ / benzene / Irradiation

3: 95 percent / dimethylsulfoxide / 50 °C

4: NaOH / methanol; H₂O / Heating

5: diethyl ether / 0 °C

6: 88 percent / NH₂OH*HCl; KOH / methanol / 0 °C

With dmap; potassium hydroxide; sodium hydroxide; hydroxylamine hydrochloride; iodine; triethylamine; In methanol; diethyl ether; dichloromethane; water; dimethyl sulfoxide; benzene;
DOI:10.1021/ol030088w

Reference yield:

: 622836-80-0
(5E,7E)-(S)-4-Benzyloxy-11-methoxymethoxy-undeca-5,7-dienenitrile

: 622836-75-3
(4S,5E,7E)-4-(benzyloxy)-N-hydroxy-11-(methoxymethoxy)undeca-5,7-dienamide

Guidance literature:: Multi-step reaction with 3 steps

1: NaOH / methanol; H₂O / Heating

2: diethyl ether / 0 °C

3: 88 percent / NH₂OH*HCl; KOH / methanol / 0 °C

With potassium hydroxide; sodium hydroxide; hydroxylamine hydrochloride; In methanol; diethyl ether; water;
DOI:10.1021/ol030088w