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C55H75N13O14

Base Information
  • Chemical Name:C55H75N13O14
  • CAS No.:1203557-35-0
  • Molecular Formula:C55H75N13O14
  • Molecular Weight:1142.28
  • Hs Code.:
C<sub>55</sub>H<sub>75</sub>N<sub>13</sub>O<sub>14</sub>

Synonyms:C55H75N13O14

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Chemical Property of C55H75N13O14
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Technology Process of C55H75N13O14

There total 13 articles about C55H75N13O14 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 10h;
DOI:10.1016/j.ejmech.2012.01.054
Guidance literature:
Multi-step reaction with 7 steps
1.1: sodium azide / N,N-dimethyl-formamide / 24 h / 60 °C
2.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.33 h / 0 °C
3.2: 25 h / 0 - 20 °C
4.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 24.67 h / 0 - 20 °C
6.1: sodium hydroxide / ethanol / 24 h / 20 °C
6.2: pH 4.5
7.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 10 h / 20 °C
With sodium azide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.01.054
Guidance literature:
Multi-step reaction with 10 steps
1.1: pyridine / 12 h / 0 - 20 °C
2.1: sodium azide / N,N-dimethyl-formamide / 24 h / 60 °C
3.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.33 h / 0 °C
4.2: 25 h / 0 - 20 °C
5.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
6.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 0 - 20 °C
7.1: diethylamine / dichloromethane / 2 h / Cooling with ice
8.1: dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane / 48 h / 20 °C
8.2: 48 h / 20 °C
9.1: trifluoroacetic acid / dichloromethane / 0.75 h / 20 °C
10.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 10 h / 20 °C
With pyridine; dmap; sodium azide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; diethylamine; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.01.054
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