trans-2-phenyl-2-thioxo-3-methyl-5-tert-butyl-1,3,2λ⁵-oxazaphosphorinane

Base Information

Chemical Name:trans-2-phenyl-2-thioxo-3-methyl-5-tert-butyl-1,3,2λ⁵-oxazaphosphorinane
CAS No.:116005-21-1
Molecular Formula:C₁₄H₂₂NOPS
Molecular Weight:283.375
Hs Code.:

trans-2-phenyl-2-thioxo-3-methyl-5-tert-butyl-1,3,2λ<sup>5</sup>-oxazaphosphorinane

Synonyms:trans-2-phenyl-2-thioxo-3-methyl-5-tert-butyl-1,3,2λ⁵-oxazaphosphorinane

Suppliers and Price of trans-2-phenyl-2-thioxo-3-methyl-5-tert-butyl-1,3,2λ⁵-oxazaphosphorinane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of trans-2-phenyl-2-thioxo-3-methyl-5-tert-butyl-1,3,2λ⁵-oxazaphosphorinane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of trans-2-phenyl-2-thioxo-3-methyl-5-tert-butyl-1,3,2λ⁵-oxazaphosphorinane

There total 3 articles about trans-2-phenyl-2-thioxo-3-methyl-5-tert-butyl-1,3,2λ⁵-oxazaphosphorinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83096-36-0
2-tert-butyl-malonic acid monoethyl ester

: 116005-21-1
trans-2-phenyl-2-thioxo-3-methyl-5-tert-butyl-1,3,2λ⁵-oxazaphosphorinane

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) thionyl chloride / 1.) reflux, 1.5 h, 2.) diethyl ether

2: 71 percent / lithium aluminum hydride / diethyl ether / 48 h / Heating

3: 632 mg / triethylamine / ethyl acetate / 48 h / Ambient temperature

With lithium aluminium tetrahydride; thionyl chloride; triethylamine; In diethyl ether; ethyl acetate;
DOI:10.1021/ja00229a027

Reference yield:

: 116005-23-3
N-methyl-2-(carbethoxy)-3,3-dimethylbutyramide

: 116005-21-1
trans-2-phenyl-2-thioxo-3-methyl-5-tert-butyl-1,3,2λ⁵-oxazaphosphorinane

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / lithium aluminum hydride / diethyl ether / 48 h / Heating

2: 632 mg / triethylamine / ethyl acetate / 48 h / Ambient temperature

With lithium aluminium tetrahydride; triethylamine; In diethyl ether; ethyl acetate;
DOI:10.1021/ja00229a027