di-tert-butyl {(3,4,5-tris{2-(2-{2-[2-methoxyethoxy]ethoxy}ethoxy)ethoxy})phenylureido}methanephosphonate

Base Information

Chemical Name:di-tert-butyl {(3,4,5-tris{2-(2-{2-[2-methoxyethoxy]ethoxy}ethoxy)ethoxy})phenylureido}methanephosphonate
CAS No.:862771-68-4
Molecular Formula:C₄₃H₈₁N₂O₁₉P
Molecular Weight:961.092
Hs Code.:

Synonyms:di-tert-butyl {(3,4,5-tris{2-(2-{2-[2-methoxyethoxy]ethoxy}ethoxy)ethoxy})phenylureido}methanephosphonate

Suppliers and Price of di-tert-butyl {(3,4,5-tris{2-(2-{2-[2-methoxyethoxy]ethoxy}ethoxy)ethoxy})phenylureido}methanephosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of di-tert-butyl {(3,4,5-tris{2-(2-{2-[2-methoxyethoxy]ethoxy}ethoxy)ethoxy})phenylureido}methanephosphonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of di-tert-butyl {(3,4,5-tris{2-(2-{2-[2-methoxyethoxy]ethoxy}ethoxy)ethoxy})phenylureido}methanephosphonate

There total 5 articles about di-tert-butyl {(3,4,5-tris{2-(2-{2-[2-methoxyethoxy]ethoxy}ethoxy)ethoxy})phenylureido}methanephosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13086-84-5
di-tert-butyl phosphite

: 862771-68-4
di-tert-butyl {(3,4,5-tris{2-(2-{2-[2-methoxyethoxy]ethoxy}ethoxy)ethoxy})phenylureido}methanephosphonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium bis(trimethylsilyl)amide / tetrahydrofuran / 0.83 h / cooling

1.2: tetrahydrofuran / 3 h

1.3: 46 percent / pentane / 0.17 h / Heating

2.1: 100 percent / N₂H₄*H₂O / ethanol / 24 Torr

3.1: 1.3 g / CH₂Cl₂ / 2 h

With potassium hexamethylsilazane; hydrazine hydrate; In tetrahydrofuran; ethanol; dichloromethane; 1.3: Arbuzov reaction;
DOI:10.1021/ja052074m

Reference yield:

: 139392-83-9
Di-tert-butyl N-phthalimidoaminomethyl phosphonate

: 862771-68-4
di-tert-butyl {(3,4,5-tris{2-(2-{2-[2-methoxyethoxy]ethoxy}ethoxy)ethoxy})phenylureido}methanephosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / N₂H₄*H₂O / ethanol / 24 Torr

2: 1.3 g / CH₂Cl₂ / 2 h

With hydrazine hydrate; In ethanol; dichloromethane;
DOI:10.1021/ja052074m

Reference yield:

: HOOC-Ph((EO)4OMe)3

: 862771-68-4
di-tert-butyl {(3,4,5-tris{2-(2-{2-[2-methoxyethoxy]ethoxy}ethoxy)ethoxy})phenylureido}methanephosphonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethyl chloroformate; Et₃N / tetrahydrofuran / 0 - 20 °C

1.2: aq. NaN₃ / tetrahydrofuran / 0 - 20 °C

2.1: toluene / 2.5 h / Heating

3.1: 1.3 g / CH₂Cl₂ / 2 h

With chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; dichloromethane; toluene; 2.1: Curtius rearrangement;
DOI:10.1021/ja052074m