4-(1-((2,5-dibromo-4-((trimethylsilyl)ethyn-2-yl)phenyl))ethyn-2-yl)-N,N-dihexylaniline

Base Information

Chemical Name:4-(1-((2,5-dibromo-4-((trimethylsilyl)ethyn-2-yl)phenyl))ethyn-2-yl)-N,N-dihexylaniline
CAS No.:1356186-33-8
Molecular Formula:C₃₁H₄₁Br₂NSi
Molecular Weight:615.567
Hs Code.:

Synonyms:4-(1-((2,5-dibromo-4-((trimethylsilyl)ethyn-2-yl)phenyl))ethyn-2-yl)-N,N-dihexylaniline

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Chemical Property of 4-(1-((2,5-dibromo-4-((trimethylsilyl)ethyn-2-yl)phenyl))ethyn-2-yl)-N,N-dihexylaniline

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Technology Process of 4-(1-((2,5-dibromo-4-((trimethylsilyl)ethyn-2-yl)phenyl))ethyn-2-yl)-N,N-dihexylaniline

There total 6 articles about 4-(1-((2,5-dibromo-4-((trimethylsilyl)ethyn-2-yl)phenyl))ethyn-2-yl)-N,N-dihexylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1356186-24-7
4-(1-(2,5-dibromo-4-iodophenyl)ethyn-2-yl)-N,N-dihexylaniline

: 1066-54-2
trimethylsilylacetylene

: 1356186-33-8
4-(1-((2,5-dibromo-4-((trimethylsilyl)ethyn-2-yl)phenyl))ethyn-2-yl)-N,N-dihexylaniline

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1039/c2cc15904j

Reference yield:

: 90134-09-1
N,N-dihexyl-4-iodobenzenamine

: 1356186-33-8
4-(1-((2,5-dibromo-4-((trimethylsilyl)ethyn-2-yl)phenyl))ethyn-2-yl)-N,N-dihexylaniline

Guidance literature:: Multi-step reaction with 4 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 12 h / 55 °C / Inert atmosphere

2: potassium carbonate / tetrahydrofuran; methanol / 2 h / 20 °C / Inert atmosphere

3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

4: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; potassium carbonate; triethylamine; In tetrahydrofuran; methanol; 1: Sonogashira coupling / 3: Sonogashira coupling / 4: Sonogashira coupling;
DOI:10.1039/c2cc15904j

Reference yield:

: 406491-06-3
N,N-dihexyl-4-ethynylaniline

: 1356186-33-8
4-(1-((2,5-dibromo-4-((trimethylsilyl)ethyn-2-yl)phenyl))ethyn-2-yl)-N,N-dihexylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; 1: Sonogashira coupling / 2: Sonogashira coupling;
DOI:10.1039/c2cc15904j