trans-4-anilino-2-2'-methylcarbamoyl-3',4'-methylenedioxyphenyl-6,7-methylenedioxy-α-tetralone

Base Information

Chemical Name:trans-4-anilino-2-2'-methylcarbamoyl-3',4'-methylenedioxyphenyl-6,7-methylenedioxy-α-tetralone
CAS No.:82464-17-3
Molecular Formula:C₂₆H₂₂N₂O₆
Molecular Weight:458.47
Hs Code.:

Synonyms:trans-4-anilino-2-2'-methylcarbamoyl-3',4'-methylenedioxyphenyl-6,7-methylenedioxy-α-tetralone

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Chemical Property of trans-4-anilino-2-2'-methylcarbamoyl-3',4'-methylenedioxyphenyl-6,7-methylenedioxy-α-tetralone

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Technology Process of trans-4-anilino-2-2'-methylcarbamoyl-3',4'-methylenedioxyphenyl-6,7-methylenedioxy-α-tetralone

There total 4 articles about trans-4-anilino-2-2'-methylcarbamoyl-3',4'-methylenedioxyphenyl-6,7-methylenedioxy-α-tetralone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 82464-25-3
4b,cis-10b,11,12-tetrahydro-4b,12-N-phenylepoxyiminooxysanguinarine

: 82464-17-3
trans-4-anilino-2-2'-methylcarbamoyl-3',4'-methylenedioxyphenyl-6,7-methylenedioxy-α-tetralone

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 0.25h; Ambient temperature;
DOI:10.1248/cpb.30.569

Reference yield:

: 22855-15-8
8-methyl-7-(6-vinyl-benzo[1,3]dioxol-5-yl)-8,9-dihydro-[1,3]dioxolo[4,5-h]isoquinoline

: 82464-17-3
trans-4-anilino-2-2'-methylcarbamoyl-3',4'-methylenedioxyphenyl-6,7-methylenedioxy-α-tetralone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) DDQ; 2.) K₃Fe(CN)6, 2.5percent aq. KOH / 1.) chloroform, room temp., 1 h.; 2.) methanol, 80 deg C, 2.5 h.

2: 77 percent / benzene / 0.17 h / Ambient temperature; Irradiation

3: 89 percent / H₂ / 10percent Pd-C / methanol / 0.25 h / Ambient temperature

With potassium hydroxide; hydrogen; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium hexacyanoferrate(III); palladium on activated charcoal; In methanol; benzene;
DOI:10.1248/cpb.30.569

Reference yield:

: 53777-79-0
N-methyl-13,14-dehydrostylopinium chloride

: 82464-17-3
trans-4-anilino-2-2'-methylcarbamoyl-3',4'-methylenedioxyphenyl-6,7-methylenedioxy-α-tetralone

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / 25percent KOH / methanol / 0.12 h / Heating

2: 1.) DDQ; 2.) K₃Fe(CN)6, 2.5percent aq. KOH / 1.) chloroform, room temp., 1 h.; 2.) methanol, 80 deg C, 2.5 h.

3: 77 percent / benzene / 0.17 h / Ambient temperature; Irradiation

4: 89 percent / H₂ / 10percent Pd-C / methanol / 0.25 h / Ambient temperature

With potassium hydroxide; hydrogen; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium hexacyanoferrate(III); palladium on activated charcoal; In methanol; benzene;
DOI:10.1248/cpb.30.569