isopropyl 10-(3-chloro-2,6-dihydroxy-5-formyl-4-methylphenyl)decanoate

Base Information

Chemical Name:isopropyl 10-(3-chloro-2,6-dihydroxy-5-formyl-4-methylphenyl)decanoate
CAS No.:1374766-75-2
Molecular Formula:C₂₁H₃₁ClO₅
Molecular Weight:398.927
Hs Code.:

Synonyms:isopropyl 10-(3-chloro-2,6-dihydroxy-5-formyl-4-methylphenyl)decanoate

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Chemical Property of isopropyl 10-(3-chloro-2,6-dihydroxy-5-formyl-4-methylphenyl)decanoate

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Technology Process of isopropyl 10-(3-chloro-2,6-dihydroxy-5-formyl-4-methylphenyl)decanoate

There total 5 articles about isopropyl 10-(3-chloro-2,6-dihydroxy-5-formyl-4-methylphenyl)decanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1374766-74-1
methyl 10-(3-chloro-5-formyl-2,6-dihydroxy-4-methylphenyl)decanoate

: 67-63-0,8013-70-5
isopropyl alcohol

: 1374766-75-2
isopropyl 10-(3-chloro-2,6-dihydroxy-5-formyl-4-methylphenyl)decanoate

Guidance literature:: With sulfuric acid; for 18h; Reflux;

Reference yield:

: 2640-94-0
methyl 10-hydroxydecanoate

: 1374766-75-2
isopropyl 10-(3-chloro-2,6-dihydroxy-5-formyl-4-methylphenyl)decanoate

Guidance literature:: Multi-step reaction with 5 steps

2: potassium hydroxide; calcium chloride / methanol

3: acetic acid; phosphoric acid

4: palladium on activated charcoal; hydrogen / ethyl acetate

5: sulfuric acid / 18 h / Reflux

With phosphoric acid; sulfuric acid; palladium on activated charcoal; hydrogen; acetic acid; calcium chloride; potassium hydroxide; In methanol; ethyl acetate; 1: |Swern Oxidation / 2: |Aldol Addition;

Reference yield:

: 14811-73-5
10-oxo-decanoic acid methyl ester

: 1374766-75-2
isopropyl 10-(3-chloro-2,6-dihydroxy-5-formyl-4-methylphenyl)decanoate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium hydroxide; calcium chloride / methanol

2: acetic acid; phosphoric acid

3: palladium on activated charcoal; hydrogen / ethyl acetate

4: sulfuric acid / 18 h / Reflux

With phosphoric acid; sulfuric acid; palladium on activated charcoal; hydrogen; acetic acid; calcium chloride; potassium hydroxide; In methanol; ethyl acetate; 1: |Aldol Addition;