tetra-tert-butyl 2-{4-[2-tert-butoxy-1-(tert-butoxycarbonyl)-2-oxoethyl]-3-nitrophenyl}propane-1,1,3,3-tetracarboxylate

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Chemical Name:tetra-tert-butyl 2-{4-[2-tert-butoxy-1-(tert-butoxycarbonyl)-2-oxoethyl]-3-nitrophenyl}propane-1,1,3,3-tetracarboxylate
CAS No.:1252576-45-6
Molecular Formula:C₄₀H₆₁NO₁₄
Molecular Weight:779.923
Hs Code.:

Synonyms:tetra-tert-butyl 2-{4-[2-tert-butoxy-1-(tert-butoxycarbonyl)-2-oxoethyl]-3-nitrophenyl}propane-1,1,3,3-tetracarboxylate

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Chemical Property of tetra-tert-butyl 2-{4-[2-tert-butoxy-1-(tert-butoxycarbonyl)-2-oxoethyl]-3-nitrophenyl}propane-1,1,3,3-tetracarboxylate

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Technology Process of tetra-tert-butyl 2-{4-[2-tert-butoxy-1-(tert-butoxycarbonyl)-2-oxoethyl]-3-nitrophenyl}propane-1,1,3,3-tetracarboxylate

There total 2 articles about tetra-tert-butyl 2-{4-[2-tert-butoxy-1-(tert-butoxycarbonyl)-2-oxoethyl]-3-nitrophenyl}propane-1,1,3,3-tetracarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 541-16-2
t-butyl malonate

: 709-58-0
1-nitro-3-(trichloromethyl)benzene

: 1252576-45-6
tetra-tert-butyl 2-{4-[2-tert-butoxy-1-(tert-butoxycarbonyl)-2-oxoethyl]-3-nitrophenyl}propane-1,1,3,3-tetracarboxylate

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 ℃; for 3h; Inert atmosphere;
DOI:10.1002/ejoc.200901303

Reference yield: 26.0%

: 541-16-2
t-butyl malonate

: 709-58-0
1-nitro-3-(trichloromethyl)benzene

: 1252576-41-2
di-tert-butyl (4-formyl-2-nitrophenyl)malonate

: 1252576-43-4
di-tert-butyl {4-[2-tert-butoxy-1-(tert-butoxycarbonyl)-2-oxoethyl]-3-nitrobenzylidene}malonate

: 1252576-45-6
tetra-tert-butyl 2-{4-[2-tert-butoxy-1-(tert-butoxycarbonyl)-2-oxoethyl]-3-nitrophenyl}propane-1,1,3,3-tetracarboxylate

Guidance literature:: t-butyl malonate; 1-nitro-3-(trichloromethyl)benzene; With potassium tert-butylate; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 ℃; for 3h; Inert atmosphere;

With hydrogenchloride; water; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200901303