Technology Process of C18H26O4
There total 7 articles about C18H26O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 0 ℃;
for 2h;
DOI:10.1021/ol200824r
- Guidance literature:
-
Multi-step reaction with 3 steps
1: manganese(IV) oxide / dichloromethane / 4 h / 0 °C
2: Raney 2400 Ni / ethanol / 12 h / 40 °C
3: sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 0 °C
With
manganese(IV) oxide; sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine;
In
ethanol; dichloromethane;
3: Parikh-Doering oxidation;
DOI:10.1021/ol200824r
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: diisobutylaluminium hydride / toluene / 1 h / -78 °C
2.1: tert.-butyl lithium / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; pentane / 0.17 h / -78 °C
2.2: 1 h / -78 °C
3.1: manganese(IV) oxide / dichloromethane / 4 h / 0 °C
4.1: Raney 2400 Ni / ethanol / 12 h / 40 °C
5.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 0 °C
With
manganese(IV) oxide; tert.-butyl lithium; sulfur trioxide pyridine complex; diisobutylaluminium hydride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; dichloromethane; toluene; pentane;
5.1: Parikh-Doering oxidation;
DOI:10.1021/ol200824r
