1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene 1-(1H-1,2,3-triazole-4-acetate)borane

Base Information

Chemical Name:1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene 1-(1H-1,2,3-triazole-4-acetate)borane
CAS No.:1377151-01-3
Molecular Formula:C₃₁H₄₂BN₅O
Molecular Weight:511.518
Hs Code.:

Synonyms:1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene 1-(1H-1,2,3-triazole-4-acetate)borane

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Chemical Property of 1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene 1-(1H-1,2,3-triazole-4-acetate)borane

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Technology Process of 1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene 1-(1H-1,2,3-triazole-4-acetate)borane

There total 2 articles about 1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene 1-(1H-1,2,3-triazole-4-acetate)borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1,3-bis-(2,6-diisopropylphenyl)imidazol-2-ylidene azidoborane

: 1423-60-5
methyl ethynyl ketone

: 1377151-01-3
1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene 1-(1H-1,2,3-triazole-4-acetate)borane

Guidance literature:: In benzene-d6; at 80 ℃; for 3.5h;
DOI:10.1021/ol300851m

Reference yield:

: 956972-12-6
1,3-bis(2,6-diiopropylphenyl)imidazol-2-ylidene borane

: 1377151-01-3
1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene 1-(1H-1,2,3-triazole-4-acetate)borane

Guidance literature:: Multi-step reaction with 2 steps

1.1: iodine / benzene / 0.25 h

1.2: 18 h

2.1: benzene-d6 / 3.5 h / 80 °C

With iodine; In benzene-d6; benzene;
DOI:10.1021/ol300851m