Technology Process of C25H30N6O5
There total 6 articles about C25H30N6O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
4-<2-(2,4-Diaminopyrrolo<2,3-d>pyrimidin-5-yl)ethyl>benzoic acid;
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
N,N-dimethyl-formamide;
for 0.166667h;
(S)-diethyl-2-amino-4-methylenepentanedionate hydrochloride;
With
triethylamine;
In
N,N-dimethyl-formamide;
for 2h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 4 A molecular sieve / triethylamine; 3-ethylbenzothiazolium bromide / ethanol / 24 h / Heating / reflux
2.1: triethylamine / methanol / 24 h / 20 °C
3.1: sodium ethanolate / ethanol
3.2: 48 h / Heating / reflux
4.1: sodium hydroxide; water / methanol / 2 h / Heating / reflux
4.2: 20 °C
5.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.17 h
5.2: 2 h
With
sodium hydroxide; 4 A molecular sieve; water; sodium ethanolate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
triethylamine; 3-ethylbenzothiazolium bromide;
In
methanol; ethanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: tetrabutyl ammonium fluoride; sodium hydrogencarbonate / palladium diacetate / toluene / 5 h / Heating / reflux
2.1: 4 A molecular sieve / triethylamine; 3-ethylbenzothiazolium bromide / ethanol / 24 h / Heating / reflux
3.1: triethylamine / methanol / 24 h / 20 °C
4.1: sodium ethanolate / ethanol
4.2: 48 h / Heating / reflux
5.1: sodium hydroxide; water / methanol / 2 h / Heating / reflux
5.2: 20 °C
6.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.17 h
6.2: 2 h
With
sodium hydroxide; 4 A molecular sieve; tetrabutyl ammonium fluoride; water; sodium ethanolate; sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
palladium diacetate; triethylamine; 3-ethylbenzothiazolium bromide;
In
methanol; ethanol; N,N-dimethyl-formamide; toluene;
