(S)-2-(((tert-butyldiphenylsilyl)oxy)methyl)-5-methoxy-3,4-dihydro-2H-pyrrole

Base Information

Chemical Name:(S)-2-(((tert-butyldiphenylsilyl)oxy)methyl)-5-methoxy-3,4-dihydro-2H-pyrrole
CAS No.:170148-26-2
Molecular Formula:C₂₂H₂₉NO₂Si
Molecular Weight:367.563
Hs Code.:

Synonyms:(S)-2-(((tert-butyldiphenylsilyl)oxy)methyl)-5-methoxy-3,4-dihydro-2H-pyrrole

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Chemical Property of (S)-2-(((tert-butyldiphenylsilyl)oxy)methyl)-5-methoxy-3,4-dihydro-2H-pyrrole

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Technology Process of (S)-2-(((tert-butyldiphenylsilyl)oxy)methyl)-5-methoxy-3,4-dihydro-2H-pyrrole

There total 4 articles about (S)-2-(((tert-butyldiphenylsilyl)oxy)methyl)-5-methoxy-3,4-dihydro-2H-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 420-37-1
trimethoxonium tetrafluoroborate

: 132974-83-5
(5S)-5-[[(tert-butyldiphenylsilyl)oxy]methyl]pyrrolidin-2-one

: 170148-26-2
(S)-2-(((tert-butyldiphenylsilyl)oxy)methyl)-5-methoxy-3,4-dihydro-2H-pyrrole

Guidance literature:: In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/anie.201901049

Reference yield: 88.0%

: 132974-83-5
(5S)-5-[[(tert-butyldiphenylsilyl)oxy]methyl]pyrrolidin-2-one

: 77-78-1
dimethyl sulfate

: 170148-26-2
(S)-2-(((tert-butyldiphenylsilyl)oxy)methyl)-5-methoxy-3,4-dihydro-2H-pyrrole

Guidance literature:: In benzene; at 60 ℃; for 18h;
DOI:10.1016/S0040-4020(03)00377-6

Reference yield:

: 17342-08-4
(S)-Pyroglutaminol

: 170148-26-2
(S)-2-(((tert-butyldiphenylsilyl)oxy)methyl)-5-methoxy-3,4-dihydro-2H-pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / imidazole / dimethylformamide / 12 h / 20 °C

2: 88 percent / benzene / 18 h / 60 °C

With 1H-imidazole; In N,N-dimethyl-formamide; benzene;
DOI:10.1016/S0040-4020(03)00377-6