5-{4-[3-chloro-4-(3-fluorobenzyloxy)phenylamino]quinazolin-6-yl}furan-2-carbaldehyde-d

Base Information

Chemical Name:5-{4-[3-chloro-4-(3-fluorobenzyloxy)phenylamino]quinazolin-6-yl}furan-2-carbaldehyde-d
CAS No.:1009307-59-8
Molecular Formula:C₂₆H₁₇ClFN₃O₃
Molecular Weight:474.883
Hs Code.:

Synonyms:5-{4-[3-chloro-4-(3-fluorobenzyloxy)phenylamino]quinazolin-6-yl}furan-2-carbaldehyde-d

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Chemical Property of 5-{4-[3-chloro-4-(3-fluorobenzyloxy)phenylamino]quinazolin-6-yl}furan-2-carbaldehyde-d

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Technology Process of 5-{4-[3-chloro-4-(3-fluorobenzyloxy)phenylamino]quinazolin-6-yl}furan-2-carbaldehyde-d

There total 1 articles about 5-{4-[3-chloro-4-(3-fluorobenzyloxy)phenylamino]quinazolin-6-yl}furan-2-carbaldehyde-d which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1009307-38-3
5-{4-[3-Chloro-4-(3-fluoro-benzyloxy)-phenylamino]-quinazolin-6-yl}-furan-2-carboxylic acid methoxy-methyl-amide

: 1009307-59-8
5-{4-[3-chloro-4-(3-fluorobenzyloxy)phenylamino]quinazolin-6-yl}furan-2-carbaldehyde-d

Guidance literature:: 5-{4-[3-Chloro-4-(3-fluoro-benzyloxy)-phenylamino]-quinazolin-6-yl}-furan-2-carboxylic acid methoxy-methyl-amide; With lithium aluminium deuteride; In tetrahydrofuran; at 0 - 5 ℃; for 1h;

With water-d2; In tetrahydrofuran;

Reference yield: 72.0%

: 1009307-59-8
5-{4-[3-chloro-4-(3-fluorobenzyloxy)phenylamino]quinazolin-6-yl}furan-2-carbaldehyde-d

: 24424-99-5
di-tert-butyl dicarbonate

: 1009307-43-0
(5-{4-[3-chloro-4-(3-fluorobenzyloxy)phenylamino]quinazolin-6-yl}furan-2-yl-methyl-d2)-(2-methanesulfonyl-1,1-d2-ethyl)carbamic acid tert-butyl ester

Guidance literature:: 2-methanesulfonyl-1,1-d2-ethylamine; 5-{4-[3-chloro-4-(3-fluorobenzyloxy)phenylamino]quinazolin-6-yl}furan-2-carbaldehyde-d; With sodium sulfate; triethylamine; In dichloromethane; at 20 ℃; for 3.16667h;

With sodium borodeuteride; In dichloromethane; at 20 ℃;

di-tert-butyl dicarbonate; With water-d2; potassium carbonate; more than 3 stages;