2,6-anhydro-7-tert-butoxycarbonylamino-7-deoxy-7-C-phenyl-L-threo-L-gulo-heptitol

Base Information

Chemical Name:2,6-anhydro-7-tert-butoxycarbonylamino-7-deoxy-7-C-phenyl-L-threo-L-gulo-heptitol
CAS No.:155158-64-8
Molecular Formula:C₁₈H₂₇NO₇
Molecular Weight:369.415
Hs Code.:

Synonyms:2,6-anhydro-7-tert-butoxycarbonylamino-7-deoxy-7-C-phenyl-L-threo-L-gulo-heptitol

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Chemical Property of 2,6-anhydro-7-tert-butoxycarbonylamino-7-deoxy-7-C-phenyl-L-threo-L-gulo-heptitol

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Technology Process of 2,6-anhydro-7-tert-butoxycarbonylamino-7-deoxy-7-C-phenyl-L-threo-L-gulo-heptitol

There total 3 articles about 2,6-anhydro-7-tert-butoxycarbonylamino-7-deoxy-7-C-phenyl-L-threo-L-gulo-heptitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 155158-63-7
2,6-anhydro-1,3,4,5-tetra-O-benzyl-7-tert-butoxycarbonylamino-7-deoxy-7-C-phenyl-L-threo-L-gulo-heptitol

: 155158-64-8
2,6-anhydro-7-tert-butoxycarbonylamino-7-deoxy-7-C-phenyl-L-threo-L-gulo-heptitol

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; ethyl acetate; for 18h;
DOI:10.1016/0008-6215(93)84163-Z

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 155158-64-8
2,6-anhydro-7-tert-butoxycarbonylamino-7-deoxy-7-C-phenyl-L-threo-L-gulo-heptitol

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / Et₃N / dioxane / 4 h / Ambient temperature

2: 93 percent / H₂ / 10percent Pd/C / ethyl acetate; methanol / 18 h

With hydrogen; triethylamine; palladium on activated charcoal; In 1,4-dioxane; methanol; ethyl acetate;
DOI:10.1016/0008-6215(93)84163-Z

Reference yield:

: (E/Z)-2,6-anhydro-3,4,5,7-tetra-O-benzyl-1-C-phenyl-D-glycero-D-ido-heptose oxime

: 155158-64-8
2,6-anhydro-7-tert-butoxycarbonylamino-7-deoxy-7-C-phenyl-L-threo-L-gulo-heptitol

Guidance literature:: Multi-step reaction with 3 steps

1: 24 percent / LiAlH₄ / tetrahydrofuran / 0.5 h / Heating

2: 90 percent / Et₃N / dioxane / 4 h / Ambient temperature

3: 93 percent / H₂ / 10percent Pd/C / ethyl acetate; methanol / 18 h

With lithium aluminium tetrahydride; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; ethyl acetate;
DOI:10.1016/0008-6215(93)84163-Z