8-nitro-3,4,5,6-tetrahydro-2H-benzo<1,4>dioxonin

Base Information

• Chemical Name: 8-nitro-3,4,5,6-tetrahydro-2H-benzo<1,4>dioxonin
• CAS No.: 135399-40-5
• Molecular Formula: C₁₁H₁₃NO₄
• Molecular Weight: 223.229

Synonyms:8-nitro-3,4,5,6-tetrahydro-2H-benzo<1,4>dioxonin

Chemical Property of 8-nitro-3,4,5,6-tetrahydro-2H-benzo<1,4>dioxonin

Chemical Property:

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Technology Process of 8-nitro-3,4,5,6-tetrahydro-2H-benzo<1,4>dioxonin

There total 1 articles about 8-nitro-3,4,5,6-tetrahydro-2H-benzo<1,4>dioxonin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

1,5-dibromo-pentane (111-24-0) + 3-nitrobenzene-1,2-diol (6665-98-1) → 8-nitro-3,4,5,6-tetrahydro-2H-benzo<1,4>dioxonin (135399-40-5)

Guidance literature:

With potassium carbonate; In i-Amyl alcohol; 1.) reflux, 4 h 2.) reflux, 4 h;

upstream raw materials:

1,5-dibromo-pentane

3-nitrobenzene-1,2-diol

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