4'-cyano-[1,1'-biphenyl]-4-yl 3-((4-(octyloxy)-2-hydroxybenzylidene)amino)benzoate

Base Information

Chemical Name:4'-cyano-[1,1'-biphenyl]-4-yl 3-((4-(octyloxy)-2-hydroxybenzylidene)amino)benzoate
CAS No.:1418291-35-6
Molecular Formula:C₃₅H₃₄N₂O₄
Molecular Weight:546.666
Hs Code.:

Synonyms:4'-cyano-[1,1'-biphenyl]-4-yl 3-((4-(octyloxy)-2-hydroxybenzylidene)amino)benzoate

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Chemical Property of 4'-cyano-[1,1'-biphenyl]-4-yl 3-((4-(octyloxy)-2-hydroxybenzylidene)amino)benzoate

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Technology Process of 4'-cyano-[1,1'-biphenyl]-4-yl 3-((4-(octyloxy)-2-hydroxybenzylidene)amino)benzoate

There total 4 articles about 4'-cyano-[1,1'-biphenyl]-4-yl 3-((4-(octyloxy)-2-hydroxybenzylidene)amino)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: C₂₂H₂₇NO₄

: 19812-93-2
4-Cyano-4'-hydroxybiphenyl

: 1418291-35-6
4'-cyano-[1,1'-biphenyl]-4-yl 3-((4-(octyloxy)-2-hydroxybenzylidene)amino)benzoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.3762/bjoc.9.4

Reference yield:

: 89027-82-7
2-hydroxy-4-(octyloxy)benzaldehyde

: 1418291-35-6
4'-cyano-[1,1'-biphenyl]-4-yl 3-((4-(octyloxy)-2-hydroxybenzylidene)amino)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / ethanol / 6 h / Reflux

2: dicyclohexyl-carbodiimide; dmap / dichloromethane / 48 h / 20 °C / Inert atmosphere

With dmap; acetic acid; dicyclohexyl-carbodiimide; In ethanol; dichloromethane;
DOI:10.3762/bjoc.9.4

Reference yield:

: 95-01-2
2,4-Dihydroxybenzaldehyde

: 1418291-35-6
4'-cyano-[1,1'-biphenyl]-4-yl 3-((4-(octyloxy)-2-hydroxybenzylidene)amino)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydrogencarbonate; potassium iodide / acetone / 48 h / Reflux

2: acetic acid / ethanol / 6 h / Reflux

3: dicyclohexyl-carbodiimide; dmap / dichloromethane / 48 h / 20 °C / Inert atmosphere

With dmap; potassium hydrogencarbonate; acetic acid; dicyclohexyl-carbodiimide; potassium iodide; In ethanol; dichloromethane; acetone;
DOI:10.3762/bjoc.9.4