3-(1,3,8,10-tetramethoxy-6,11-dihydrodibenzo[b,e]oxepin-11-yl)-1-tosyl-1H-indole

Base Information

• Chemical Name: 3-(1,3,8,10-tetramethoxy-6,11-dihydrodibenzo[b,e]oxepin-11-yl)-1-tosyl-1H-indole
• CAS No.: 1298072-01-1
• Molecular Formula: C₃₃H₃₁NO₇S
• Molecular Weight: 585.678

Synonyms:3-(1,3,8,10-tetramethoxy-6,11-dihydrodibenzo[b,e]oxepin-11-yl)-1-tosyl-1H-indole

Chemical Property of 3-(1,3,8,10-tetramethoxy-6,11-dihydrodibenzo[b,e]oxepin-11-yl)-1-tosyl-1H-indole

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 3-(1,3,8,10-tetramethoxy-6,11-dihydrodibenzo[b,e]oxepin-11-yl)-1-tosyl-1H-indole

There total 3 articles about 3-(1,3,8,10-tetramethoxy-6,11-dihydrodibenzo[b,e]oxepin-11-yl)-1-tosyl-1H-indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1-(4-tolylsulfonyl)indole-3-carboxaldehyde (50562-79-3) + 1-(3,5-dimethoxybenzyloxy)-3,5-dimethoxybenzene (22216-25-7) → 3-(1,3,8,10-tetramethoxy-6,11-dihydrodibenzo[b,e]oxepin-11-yl)-1-tosyl-1H-indole (1298072-01-1)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 9h; Inert atmosphere;

DOI:10.1002/ejoc.201001739

Reference yield:

3,5-dimethoxyphenol (500-99-2) → 3-(1,3,8,10-tetramethoxy-6,11-dihydrodibenzo[b,e]oxepin-11-yl)-1-tosyl-1H-indole (1298072-01-1)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2: boron trifluoride diethyl etherate / dichloromethane / 9 h / 20 °C / Inert atmosphere

With boron trifluoride diethyl etherate; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1002/ejoc.201001739

Reference yield:

3,5-dimethoxybenzyl bromide (877-88-3) → 3-(1,3,8,10-tetramethoxy-6,11-dihydrodibenzo[b,e]oxepin-11-yl)-1-tosyl-1H-indole (1298072-01-1)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

2: boron trifluoride diethyl etherate / dichloromethane / 9 h / 20 °C / Inert atmosphere

With boron trifluoride diethyl etherate; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1002/ejoc.201001739

upstream raw materials:

3,5-dimethoxyphenol

1-(4-tolylsulfonyl)indole-3-carboxaldehyde

1-(3,5-dimethoxybenzyloxy)-3,5-dimethoxybenzene

3,5-dimethoxybenzyl bromide

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