(3-benzyl-2-exo-methyl-7-exo-pyrrolidin-1-yl-3-azabicyclo[3.2.0]hept-6-endo-yl)methanol

Base Information

Chemical Name:(3-benzyl-2-exo-methyl-7-exo-pyrrolidin-1-yl-3-azabicyclo[3.2.0]hept-6-endo-yl)methanol
CAS No.:1400914-19-3
Molecular Formula:C₁₉H₂₈N₂O
Molecular Weight:300.444
Hs Code.:

Synonyms:(3-benzyl-2-exo-methyl-7-exo-pyrrolidin-1-yl-3-azabicyclo[3.2.0]hept-6-endo-yl)methanol

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Chemical Property of (3-benzyl-2-exo-methyl-7-exo-pyrrolidin-1-yl-3-azabicyclo[3.2.0]hept-6-endo-yl)methanol

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Technology Process of (3-benzyl-2-exo-methyl-7-exo-pyrrolidin-1-yl-3-azabicyclo[3.2.0]hept-6-endo-yl)methanol

There total 3 articles about (3-benzyl-2-exo-methyl-7-exo-pyrrolidin-1-yl-3-azabicyclo[3.2.0]hept-6-endo-yl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: lipase B of Candida antarctica

: (3-benzyl-2-exo-methyl-7-exo-pyrrolidin-1-yl-3-azabicyclo[3.2.0]hept-6-endo-yl)methanol

: 1400914-19-3
(3-benzyl-2-exo-methyl-7-exo-pyrrolidin-1-yl-3-azabicyclo[3.2.0]hept-6-endo-yl)methanol

: C₂₁H₃₀N₂O₂

Guidance literature:: In ethyl acetate; at 20 ℃; Inert atmosphere; Enzymatic reaction;
DOI:10.1016/j.ejmech.2012.07.025

Reference yield:

: C₂₁H₃₀N₂O₂

: 1400914-19-3
(3-benzyl-2-exo-methyl-7-exo-pyrrolidin-1-yl-3-azabicyclo[3.2.0]hept-6-endo-yl)methanol

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran; dichloromethane / 3 h / Molecular sieve; Inert atmosphere

2: ethyl acetate / 20 °C / Inert atmosphere; Enzymatic reaction

With lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1016/j.ejmech.2012.07.025

Reference yield:

: 129975-11-7
ethyl N-benzylaminocrotonate

: 1400914-19-3
(3-benzyl-2-exo-methyl-7-exo-pyrrolidin-1-yl-3-azabicyclo[3.2.0]hept-6-endo-yl)methanol

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 20 °C / Molecular sieve; Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran; dichloromethane / 3 h / Molecular sieve; Inert atmosphere

3: ethyl acetate / 20 °C / Inert atmosphere; Enzymatic reaction

With lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1016/j.ejmech.2012.07.025