6-methoxy-2-(4-methoxyphenyl)-3-[4-(N-methyl-N-2-(piperidin-1-yl)ethylamino)benzoyl]-benzo[b]thiophene

Base Information

• Chemical Name: 6-methoxy-2-(4-methoxyphenyl)-3-[4-(N-methyl-N-2-(piperidin-1-yl)ethylamino)benzoyl]-benzo[b]thiophene
• CAS No.: 206434-71-1
• Molecular Formula: C₃₁H₃₄N₂O₃S
• Molecular Weight: 514.689

Synonyms:6-methoxy-2-(4-methoxyphenyl)-3-[4-(N-methyl-N-2-(piperidin-1-yl)ethylamino)benzoyl]-benzo[b]thiophene

Chemical Property of 6-methoxy-2-(4-methoxyphenyl)-3-[4-(N-methyl-N-2-(piperidin-1-yl)ethylamino)benzoyl]-benzo[b]thiophene

Chemical Property:

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Technology Process of 6-methoxy-2-(4-methoxyphenyl)-3-[4-(N-methyl-N-2-(piperidin-1-yl)ethylamino)benzoyl]-benzo[b]thiophene

There total 6 articles about 6-methoxy-2-(4-methoxyphenyl)-3-[4-(N-methyl-N-2-(piperidin-1-yl)ethylamino)benzoyl]-benzo[b]thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

MeCl2 + 4-[(N-methyl-N-(2-piperidin-1-yl)-ethyl)amino]benzoic acid + 2-(4'-methoxyphenyl)-6-methoxybenzothiophene (63675-74-1) → 6-methoxy-2-(4-methoxyphenyl)-3-[4-(N-methyl-N-2-(piperidin-1-yl)ethylamino)benzoyl]-benzo[b]thiophene (206434-71-1)

Guidance literature:

With thionyl chloride; AlCl₃; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

4-[(N-methyl-N-(2-piperidin-l-yl)ethyl)amino]benzoic acid + MeCl2 + 2-(4'-methoxyphenyl)-6-methoxybenzothiophene (63675-74-1) → 6-methoxy-2-(4-methoxyphenyl)-3-[4-(N-methyl-N-2-(piperidin-1-yl)ethylamino)benzoyl]-benzo[b]thiophene (206434-71-1)

Guidance literature:

With thionyl chloride; AlCl₃; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

2-(4'-methoxyphenyl)-6-methoxybenzothiophene (63675-74-1) + 4-[methyl-(2-piperidin-1-yl-ethyl)-amino]-benzoyl chloride (206434-82-4) → 6-methoxy-2-(4-methoxyphenyl)-3-[4-(N-methyl-N-2-(piperidin-1-yl)ethylamino)benzoyl]-benzo[b]thiophene (206434-71-1)

Guidance literature:

With aluminium trichloride; In 1,2-dichloro-ethane; at 5 - 23 ℃; Yield given;

DOI:10.1016/S0960-894X(99)00050-5

upstream raw materials:

2-(4'-methoxyphenyl)-6-methoxybenzothiophene

4-[methyl-(2-piperidin-1-yl-ethyl)-amino]-benzoyl chloride

methyl 4-(N-methyl)aminobenzoate

4-[methyl-(2-piperidin-1-yl-ethyl)-amino]-benzoic acid methyl ester

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