3-{(4-[N,N-bis(2-{N',N'-bis[(ethoxycarbonyl)methyl]amino}ethyl)amino]-4-ethoxycarbonyl)-butan-1-yl}phenylpropionic acid

Base Information

Chemical Name:3-{(4-[N,N-bis(2-{N',N'-bis[(ethoxycarbonyl)methyl]amino}ethyl)amino]-4-ethoxycarbonyl)-butan-1-yl}phenylpropionic acid
CAS No.:1290118-60-3
Molecular Formula:C₃₆H₅₇N₃O₁₂
Molecular Weight:723.861
Hs Code.:

Synonyms:3-{(4-[N,N-bis(2-{N',N'-bis[(ethoxycarbonyl)methyl]amino}ethyl)amino]-4-ethoxycarbonyl)-butan-1-yl}phenylpropionic acid

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Chemical Property of 3-{(4-[N,N-bis(2-{N',N'-bis[(ethoxycarbonyl)methyl]amino}ethyl)amino]-4-ethoxycarbonyl)-butan-1-yl}phenylpropionic acid

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Technology Process of 3-{(4-[N,N-bis(2-{N',N'-bis[(ethoxycarbonyl)methyl]amino}ethyl)amino]-4-ethoxycarbonyl)-butan-1-yl}phenylpropionic acid

There total 3 articles about 3-{(4-[N,N-bis(2-{N',N'-bis[(ethoxycarbonyl)methyl]amino}ethyl)amino]-4-ethoxycarbonyl)-butan-1-yl}phenylpropionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 3-{(4-[N,N-bis(2-{N',N'-bis[(ethoxycarbonyl)methyl]amino}ethyl)amino]4-ethoxycarbonyl)-buten-1-yl}phenylpropionic acid

: 1290118-60-3
3-{(4-[N,N-bis(2-{N',N'-bis[(ethoxycarbonyl)methyl]amino}ethyl)amino]-4-ethoxycarbonyl)-butan-1-yl}phenylpropionic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; for 13.5h;

Reference yield:

: 1290118-42-1
tetraethyl 2,2',2'',2'''-(2,2'-(1-ethoxy-1-oxopent-4-en-2-ylazanediyl)bis(ethane-2,1-diyl))bis(azanetriyl)tetraacetate

: 1290118-60-3
3-{(4-[N,N-bis(2-{N',N'-bis[(ethoxycarbonyl)methyl]amino}ethyl)amino]-4-ethoxycarbonyl)-butan-1-yl}phenylpropionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / PdCl₂(MeCN)₂ / N,N-dimethyl-formamide; water / 4.5 h / 60 °C

2: hydrogen / palladium on activated charcoal / 13.5 h

With hydrogen; N-ethyl-N,N-diisopropylamine; PdCl₂(MeCN)₂; palladium on activated charcoal; In water; N,N-dimethyl-formamide;

Reference yield:

: 51992-77-9
pentaethyl diethylenetriamine-N,N,N',N'',N''-pentaacetate

: 1290118-60-3
3-{(4-[N,N-bis(2-{N',N'-bis[(ethoxycarbonyl)methyl]amino}ethyl)amino]-4-ethoxycarbonyl)-butan-1-yl}phenylpropionic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: N,N-dimethyl-formamide / 39 h / 20 - 40 °C

1.2: 70 h / 80 °C

2.1: N-ethyl-N,N-diisopropylamine / PdCl₂(MeCN)₂ / N,N-dimethyl-formamide; water / 4.5 h / 60 °C

3.1: hydrogen / palladium on activated charcoal / 13.5 h

With hydrogen; N-ethyl-N,N-diisopropylamine; PdCl₂(MeCN)₂; palladium on activated charcoal; In water; N,N-dimethyl-formamide;