closo-6,6-(di(but-3-enyl)phenylphosphine)2-6,2,3-RuC₂B₇H₉

Base Information

Chemical Name:closo-6,6-(di(but-3-enyl)phenylphosphine)2-6,2,3-RuC₂B₇H₉
CAS No.:74108-30-8
Molecular Formula:C₃₀H₄₇B₇P₂Ru
Molecular Weight:646.398
Hs Code.:

closo-6,6-(di(but-3-enyl)phenylphosphine)2-6,2,3-RuC<sub>2</sub>B<sub>7</sub>H<sub>9</sub>

Synonyms:closo-6,6-(di(but-3-enyl)phenylphosphine)2-6,2,3-RuC₂B₇H₉

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of closo-6,6-(di(but-3-enyl)phenylphosphine)2-6,2,3-RuC₂B₇H₉

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Technology Process of closo-6,6-(di(but-3-enyl)phenylphosphine)2-6,2,3-RuC₂B₇H₉

There total 1 articles about closo-6,6-(di(but-3-enyl)phenylphosphine)2-6,2,3-RuC₂B₇H₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 61081-79-6
hyper-closo-6,6-[P(C₆H₅)3]2-6,2,3-RuC₂B₇H₉

: 26681-85-6
di(but-3-enyl)phenylphosphine

: 74108-30-8
closo-6,6-(di(but-3-enyl)phenylphosphine)2-6,2,3-RuC₂B₇H₉

Guidance literature:: In toluene; byproducts: P(C6H5)3; (N2 or Ar); P-compound added to a stirred suspn. of Ru-complex; layered with pentane; allowed to stand overnight; cooled to -15°C for 2 days; pptd.; filtered in air; washed with methanol and petroleumether; dried in vacuo; elem. anal.;
DOI:10.1021/ja00538a014

Reference yield: 87.0%

: 74108-30-8
closo-6,6-(di(but-3-enyl)phenylphosphine)2-6,2,3-RuC₂B₇H₉

: 74108-31-9
closo-6-CO-6,6-(di(but-3-enyl)phenylphosphine)2-6,2,3-RuC₂B₇H₉

Guidance literature:: With CO; In toluene; (N2 or Ar); CO bubbled through a soln. of Ru-complex; petroleum ether added; cooled to -15°C for 1 day; elem. anal.;
DOI:10.1021/ja00538a014