C₆₀H₉₀N₄O₁₂

Base Information

• Chemical Name: C₆₀H₉₀N₄O₁₂
• CAS No.: 1400575-63-4
• Molecular Formula: C₆₀H₉₀N₄O₁₂
• Molecular Weight: 1059.39
• Mol file: 1400575-63-4.mol

Synonyms:C₆₀H₉₀N₄O₁₂

Chemical Property of C₆₀H₉₀N₄O₁₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₆₀H₉₀N₄O₁₂

There total 1 articles about C₆₀H₉₀N₄O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

methyl-5-amino-2-(octyloxy)benzoate + N,N'-bis(carboxymethyl)-4,6-bis(octyloxy)-1,3-benzenedicarboxamide (267897-60-9) → C60H90N4O12 (1400575-63-4)

Guidance literature:

With palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In tetrahydrofuran; at 70 ℃; for 50h;

DOI:10.1016/j.bmcl.2012.08.053

Reference yield: 93.0%

C60H90N4O12 (1400575-63-4) → C58H86N4O12 (1400575-64-5)

Guidance literature:

With water; sodium hydroxide; In tetrahydrofuran; Inert atmosphere; Reflux;

DOI:10.1039/c2cc35004a

Reference yield:

C60H90N4O12 (1400575-63-4) → C80H128N6O11

Guidance literature:

Multi-step reaction with 2 steps

1.1: water; sodium hydroxide / tetrahydrofuran / Inert atmosphere; Reflux

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 1 h / Inert atmosphere

2.2: 20 °C / Inert atmosphere

With water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In tetrahydrofuran; dichloromethane;

DOI:10.1039/c2cc35004a

upstream raw materials:

N,N'-bis(carboxymethyl)-4,6-bis(octyloxy)-1,3-benzenedicarboxamide

Downstream raw materials:

C₅₈H₈₆N₄O₁₂