11-(4-chlorophenyl)-7,8,9,10-tetrahydro[1,2,3]triazino[4',5':4,5]thieno[2,3-b]quinolin-4-yl methyl sulfide

Base Information

Chemical Name:11-(4-chlorophenyl)-7,8,9,10-tetrahydro[1,2,3]triazino[4',5':4,5]thieno[2,3-b]quinolin-4-yl methyl sulfide
CAS No.:135300-28-6
Molecular Formula:C₁₉H₁₅ClN₄S₂
Molecular Weight:398.94
Hs Code.:

Synonyms:4-methylthio-11-p-chlorophenyl-7,8,9,10-tetrahydro-quinolino<3',2':4,5>thieno<3,2-d>-1,2,3-triazine

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Chemical Property of 11-(4-chlorophenyl)-7,8,9,10-tetrahydro[1,2,3]triazino[4',5':4,5]thieno[2,3-b]quinolin-4-yl methyl sulfide

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Technology Process of 11-(4-chlorophenyl)-7,8,9,10-tetrahydro[1,2,3]triazino[4',5':4,5]thieno[2,3-b]quinolin-4-yl methyl sulfide

There total 2 articles about 11-(4-chlorophenyl)-7,8,9,10-tetrahydro[1,2,3]triazino[4',5':4,5]thieno[2,3-b]quinolin-4-yl methyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 94833-68-8
3-amino-4-(p-chlorophenyl)-5,6,7,8-tetrahydrothieno<2,3-b>quinoline-2-carbonitrile

: 135300-28-6
4-methylthio-11-p-chlorophenyl-7,8,9,10-tetrahydro-quinolino<3',2':4,5>thieno<3,2-d>-1,2,3-triazine

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / CH₃COOH, conc. HCl, NaNO₂ / H₂O / 2 h

2: 91 percent / thiourea / methanol / 3 h / Heating

3: 83 percent / 5percent NaOH / 2 h

With hydrogenchloride; sodium hydroxide; acetic acid; thiourea; sodium nitrite; In methanol; water;

Reference yield:

: 135300-22-0
4-chloro-11-p-chlorophenyl-7,8,9,10-tetrahydro-quinolino<3',2':4,5>thieno<3,2-d>-1,2,3-triazine

: 135300-28-6
4-methylthio-11-p-chlorophenyl-7,8,9,10-tetrahydro-quinolino<3',2':4,5>thieno<3,2-d>-1,2,3-triazine

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / thiourea / methanol / 3 h / Heating

2: 83 percent / 5percent NaOH / 2 h

With sodium hydroxide; thiourea; In methanol;