[N-(1,3-dimesitylimidazol-2-ylidene)-N'-(p-tolyl)thioureato]palladium allyl

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Chemical Name:[N-(1,3-dimesitylimidazol-2-ylidene)-N'-(p-tolyl)thioureato]palladium allyl
CAS No.:1434000-07-3
Molecular Formula:C₃₂H₃₆N₄PdS
Molecular Weight:615.151
Hs Code.:

Synonyms:[N-(1,3-dimesitylimidazol-2-ylidene)-N'-(p-tolyl)thioureato]palladium allyl

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Chemical Property of [N-(1,3-dimesitylimidazol-2-ylidene)-N'-(p-tolyl)thioureato]palladium allyl

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Technology Process of [N-(1,3-dimesitylimidazol-2-ylidene)-N'-(p-tolyl)thioureato]palladium allyl

There total 2 articles about [N-(1,3-dimesitylimidazol-2-ylidene)-N'-(p-tolyl)thioureato]palladium allyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: bis(η3-allyl-μ-chloropalladium(II))

: 1434000-04-0
N-(1,3-dimesitylimidazol-2-ylidene)-N'-(p-tolyl)thiourea

: 1434000-07-3
[N-(1,3-dimesitylimidazol-2-ylidene)-N'-(p-tolyl)thioureato]palladium allyl

Guidance literature:: N-(1,3-dimesitylimidazol-2-ylidene)-N'-(p-tolyl)thiourea; With sodium hexamethyldisilazane; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

bis(η3-allyl-μ-chloropalladium(II)); In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/om400220v

Reference yield:

: 1,3-bis(2,4,6-trimethylphenyl)imidazolin-2-imine

: 1434000-07-3
[N-(1,3-dimesitylimidazol-2-ylidene)-N'-(p-tolyl)thioureato]palladium allyl

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 4 h / 20 °C / Inert atmosphere

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2.2: 2 h / 20 °C / Inert atmosphere

With sodium hexamethyldisilazane; In tetrahydrofuran; dichloromethane;
DOI:10.1021/om400220v