N-(4-chlorophenyl)-2-(1-methyl-4-nitro-1H-pyrrole-2-carbonyl)hydrazine carboxamide

Base Information

Chemical Name:N-(4-chlorophenyl)-2-(1-methyl-4-nitro-1H-pyrrole-2-carbonyl)hydrazine carboxamide
CAS No.:1616260-89-9
Molecular Formula:C₁₃H₁₂ClN₅O₄
Molecular Weight:337.722
Hs Code.:

Synonyms:N-(4-chlorophenyl)-2-(1-methyl-4-nitro-1H-pyrrole-2-carbonyl)hydrazine carboxamide

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Chemical Property of N-(4-chlorophenyl)-2-(1-methyl-4-nitro-1H-pyrrole-2-carbonyl)hydrazine carboxamide

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Technology Process of N-(4-chlorophenyl)-2-(1-methyl-4-nitro-1H-pyrrole-2-carbonyl)hydrazine carboxamide

There total 4 articles about N-(4-chlorophenyl)-2-(1-methyl-4-nitro-1H-pyrrole-2-carbonyl)hydrazine carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 104-12-1
p-chlorphenylisocyanate

: 28494-50-0
1-methyl-4-nitropyrrole-2-carboxylic acid hydrazide

: 1616260-89-9
N-(4-chlorophenyl)-2-(1-methyl-4-nitro-1H-pyrrole-2-carbonyl)hydrazine carboxamide

Guidance literature:: In ethanol; N,N-dimethyl-formamide; Inert atmosphere; Reflux;
DOI:10.1016/j.bmcl.2014.05.018

Reference yield:

: 96-54-8
N-Methylpyrrole

: 1616260-89-9
N-(4-chlorophenyl)-2-(1-methyl-4-nitro-1H-pyrrole-2-carbonyl)hydrazine carboxamide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / diethyl ether

2: nitric acid; acetic anhydride / 2 h / -10 °C

3: hydrazine hydrate / ethanol / 2 h / 20 °C

4: ethanol; N,N-dimethyl-formamide / Inert atmosphere; Reflux

With nitric acid; acetic anhydride; potassium carbonate; hydrazine hydrate; In diethyl ether; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.05.018

Reference yield:

: 21898-65-7
1-methyl-2-trichloroacetyl-1H-pyrrole

: 1616260-89-9
N-(4-chlorophenyl)-2-(1-methyl-4-nitro-1H-pyrrole-2-carbonyl)hydrazine carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: nitric acid; acetic anhydride / 2 h / -10 °C

2: hydrazine hydrate / ethanol / 2 h / 20 °C

3: ethanol; N,N-dimethyl-formamide / Inert atmosphere; Reflux

With nitric acid; acetic anhydride; hydrazine hydrate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.05.018