C₂₅H₂₅F₃N₂O₆S

Base Information

Chemical Name:C₂₅H₂₅F₃N₂O₆S
CAS No.:1355686-27-9
Molecular Formula:C₂₅H₂₅F₃N₂O₆S
Molecular Weight:538.545
Hs Code.:

C<sub>25</sub>H<sub>25</sub>F<sub>3</sub>N<sub>2</sub>O<sub>6</sub>S

Synonyms:C₂₅H₂₅F₃N₂O₆S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₂₅F₃N₂O₆S

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Technology Process of C₂₅H₂₅F₃N₂O₆S

There total 6 articles about C₂₅H₂₅F₃N₂O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1355686-25-7
C₂₇H₂₇F₃N₂O₇S

: 1355686-27-9
C₂₅H₂₅F₃N₂O₆S

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 2h;

Reference yield:

: 21320-91-2
2-methoxy-4-nitrobenzene-1-sulfonyl chloride

: 1355686-27-9
C₂₅H₂₅F₃N₂O₆S

Guidance literature:: Multi-step reaction with 6 steps

1.1: ammonia / water / 72 h / 20 °C

2.1: palladium 10% on activated carbon; hydrogen / methanol; ethyl acetate / 2 h / 20 °C

3.1: sodium nitrite; hydrogenchloride / water / 3 h / Cooling with ice

3.2: 0.5 h / 20 - 70 °C

4.1: hydrogenchloride / water / 3 h / 120 °C

5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 24 h / 20 °C

6.1: sodium hydroxide / methanol; tetrahydrofuran / 2 h / 20 °C

With hydrogenchloride; palladium 10% on activated carbon; ammonia; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; sodium nitrite; In tetrahydrofuran; methanol; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 746630-16-0
2-methoxy-4-nitrobenzenesulfonamide

: 1355686-27-9
C₂₅H₂₅F₃N₂O₆S

Guidance literature:: Multi-step reaction with 5 steps

1.1: palladium 10% on activated carbon; hydrogen / methanol; ethyl acetate / 2 h / 20 °C

2.1: sodium nitrite; hydrogenchloride / water / 3 h / Cooling with ice

2.2: 0.5 h / 20 - 70 °C

3.1: hydrogenchloride / water / 3 h / 120 °C

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 24 h / 20 °C

5.1: sodium hydroxide / methanol; tetrahydrofuran / 2 h / 20 °C

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; sodium nitrite; In tetrahydrofuran; methanol; water; ethyl acetate; N,N-dimethyl-formamide;