Trichlor(4-methoxyphenyl)methylphosphoran

Base Information

Chemical Name:Trichlor(4-methoxyphenyl)methylphosphoran
CAS No.:68344-18-3
Molecular Formula:C₈H₁₀Cl₃OP
Molecular Weight:259.5
Hs Code.:

Synonyms:Trichlor(4-methoxyphenyl)methylphosphoran

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Chemical Property of Trichlor(4-methoxyphenyl)methylphosphoran

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Technology Process of Trichlor(4-methoxyphenyl)methylphosphoran

There total 3 articles about Trichlor(4-methoxyphenyl)methylphosphoran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: Dichlor(4-methoxyphenyl)methylphosphonium-hydrogendichlorid

: 68344-18-3
Trichlor(4-methoxyphenyl)methylphosphoran

Guidance literature:: With argon; In chloroform; for 0.5h; Heating;

Reference yield:

: 17847-88-0
(4-Methoxyphenyl)methyldithiophosphinsaeure

: 68344-18-3
Trichlor(4-methoxyphenyl)methylphosphoran

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / 50-100 mmol/h Cl₂ / CCl₄ / 1) 0 deg C, 2) r.t., 30 min

2: 96 percent / Ar / CHCl₃ / 0.5 h / Heating

With 50-100 mmol; argon; chlorine; In tetrachloromethane; chloroform;

Reference yield:

: Ammonium-(4-methoxyphenyl)methyldithiophosphinat

: 68344-18-3
Trichlor(4-methoxyphenyl)methylphosphoran

Guidance literature:: Multi-step reaction with 2 steps

1: 1) Cl₂, 2) HCl / 1) CCl₄, 0 deg C, 2) CCl₄, 15 min

2: 96 percent / Ar / CHCl₃ / 0.5 h / Heating

With hydrogenchloride; argon; chlorine; In chloroform;