methyl p-aminooxybenzoate

Base Information

Chemical Name:methyl p-aminooxybenzoate
CAS No.:128080-16-0
Molecular Formula:C₈H₉NO₃
Molecular Weight:167.164
Hs Code.:

Synonyms:methyl p-aminooxybenzoate

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Chemical Property of methyl p-aminooxybenzoate

Chemical Property:

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Technology Process of methyl p-aminooxybenzoate

There total 2 articles about methyl p-aminooxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99768-12-4
4-methoxycarbonylphenylboronic acid

: 128080-16-0
methyl p-aminooxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) chloride; pyridine / 1,2-dichloro-ethane / 20 °C / Molecular sieve

2: hydrazine hydrate / methanol; chloroform / 20 °C / Inert atmosphere

With pyridine; hydrazine hydrate; copper(l) chloride; In methanol; chloroform; 1,2-dichloro-ethane;
DOI:10.1039/c4cc05485g

Reference yield:

: 99-76-3,156291-94-0
methyl 4-hydroxylbenzoate

: 128080-16-0
methyl p-aminooxybenzoate

Guidance literature:: methyl 4-hydroxylbenzoate; With sodium methylate; In methanol; at 20 ℃; for 0.5h; Inert atmosphere;

With mesitylenesulfonylhydroxylamine; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere; Cooling with ice;
DOI:10.1002/adsc.201601296

Reference yield: 38.0%

: 128080-16-0
methyl p-aminooxybenzoate

: 7352-28-5
N-(benzyloxycarbonyl)-L-valyl-L-threonine methyl ester

: 1159180-80-9
C₂₆H₃₁N₃O₈

: 1159180-79-6
C₂₆H₃₁N₃O₉

Guidance literature:: N-(benzyloxycarbonyl)-L-valyl-L-threonine methyl ester; In acetonitrile; at 45 ℃;

methyl p-aminooxybenzoate; With hydrogenchloride; In dimethyl sulfoxide;
DOI:10.1016/j.tetlet.2009.03.107