1-bromo-4-tert-butyldimethylsilyloxy-2,6-dimethoxy-3,5-dimethylbenzene

Base Information

Chemical Name:1-bromo-4-tert-butyldimethylsilyloxy-2,6-dimethoxy-3,5-dimethylbenzene
CAS No.:1080023-55-7
Molecular Formula:C₁₆H₂₇BrO₃Si
Molecular Weight:375.378
Hs Code.:

Synonyms:1-bromo-4-tert-butyldimethylsilyloxy-2,6-dimethoxy-3,5-dimethylbenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-bromo-4-tert-butyldimethylsilyloxy-2,6-dimethoxy-3,5-dimethylbenzene

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Technology Process of 1-bromo-4-tert-butyldimethylsilyloxy-2,6-dimethoxy-3,5-dimethylbenzene

There total 1 articles about 1-bromo-4-tert-butyldimethylsilyloxy-2,6-dimethoxy-3,5-dimethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1080023-53-5
4-bromo-3,5-dimethoxy-2,6-dimethylphenol

: 69739-34-0
t-butyldimethylsiyl triflate

: 1080023-55-7
1-bromo-4-tert-butyldimethylsilyloxy-2,6-dimethoxy-3,5-dimethylbenzene

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1021/ol802183p

Reference yield: 62.0%

: 96-17-3,57456-98-1
2-Methylbutyraldehyde

: 1080023-55-7
1-bromo-4-tert-butyldimethylsilyloxy-2,6-dimethoxy-3,5-dimethylbenzene

: 1080023-59-1
3-tert-butyldimethylsilyloxy-1,5-dimethoxy-2,4-dimethylbenzene

: 1080023-56-8
1-(4-tert-butyldimethylsilyloxy-2,6-dimethoxy-3,5-dimethylphenyl)-2-methylbutan-1-ol

Guidance literature:: 1-bromo-4-tert-butyldimethylsilyloxy-2,6-dimethoxy-3,5-dimethylbenzene; With tert.-butyl lithium; In pentane; at -78 - -10 ℃;

2-Methylbutyraldehyde; In pentane; at -78 - 20 ℃;
DOI:10.1021/ol802183p