(+/-)-5-hydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-3-oxohexanoic acid decyl ester

Base Information

Chemical Name:(+/-)-5-hydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-3-oxohexanoic acid decyl ester
CAS No.:1051966-60-9
Molecular Formula:C₂₈H₄₄O₅S₂
Molecular Weight:524.786
Hs Code.:

Synonyms:(+/-)-5-hydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-3-oxohexanoic acid decyl ester

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Chemical Property of (+/-)-5-hydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-3-oxohexanoic acid decyl ester

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Technology Process of (+/-)-5-hydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-3-oxohexanoic acid decyl ester

There total 1 articles about (+/-)-5-hydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-3-oxohexanoic acid decyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 112-30-1
1-Decanol

: 1051966-45-0
(+/-)-6-(2-hydroxy-3-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]-dithian-2-yl}-propyl)-2,2-dimethyl-[1,3]-dioxin-4-one

: 1051966-60-9
(+/-)-5-hydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-3-oxohexanoic acid decyl ester

Guidance literature:: In toluene; at 110 ℃; for 6h;
DOI:10.1021/jm8007322

Reference yield: 79.0%

: 1051966-60-9
(+/-)-5-hydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-3-oxohexanoic acid decyl ester

: (+/-)-(3R*,5R*)-3,5-dihydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-hexanoic acid decyl ester

Guidance literature:: With tetramethylammonium triacetoxyborohydride; In dichloromethane; acetic acid; ethyl acetate; acetonitrile; at 0 ℃; for 3h;

Reference yield:

: 1051966-60-9
(+/-)-5-hydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-3-oxohexanoic acid decyl ester

: (+/-)-(3R*5S*)-3,5-dihydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-hexanoic acid decyl ester

: (+/-)-(3R*,5R*)-3,5-dihydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-hexanoic acid decyl ester

Guidance literature:: With acetic acid; tetramethylammonium triacetoxyborohydride; In methanol; dichloromethane; acetonitrile; at 0 ℃; for 2h; optical yield given as %de;
DOI:10.1021/jm8007322