1-(4-methoxyphenyl)ethenyl methyl carbonate

Base Information

• Chemical Name: 1-(4-methoxyphenyl)ethenyl methyl carbonate
• CAS No.: 146335-19-5
• Molecular Formula: C₁₁H₁₂O₄
• Molecular Weight: 208.214
• Mol file: 146335-19-5.mol

Synonyms:1-(4-methoxyphenyl)ethenyl methyl carbonate

Chemical Property of 1-(4-methoxyphenyl)ethenyl methyl carbonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(4-methoxyphenyl)ethenyl methyl carbonate

There total 1 articles about 1-(4-methoxyphenyl)ethenyl methyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

methyl chloroformate (79-22-1) + 2-Bromo-4'-methoxyacetophenone (2632-13-5) → 1-(4-methoxyphenyl)ethenyl methyl carbonate (146335-19-5)

Guidance literature:

With tetrabutylammonium tetrafluoroborate; In dichloromethane; at 15 ℃; electrochemical red.: Hg cathode, -0.6 V;

DOI:10.1055/s-1992-26339

Reference yield: 90.0%

1-(4-methoxyphenyl)ethenyl methyl carbonate (146335-19-5) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 2-Oxo-2-(4-methoxyphenyl)ethyl formate (171119-05-4)

Guidance literature:

With lithium perchlorate; at 15 ℃; electrolysis: anode: carbon, cathode: stainless steel, +1.5 V vs SCE;

DOI:10.1021/jo00122a056

upstream raw materials:

methyl chloroformate

2-Bromo-4'-methoxyacetophenone

Downstream raw materials:

2-Oxo-2-(4-methoxyphenyl)ethyl formate