2'-O-bis(phenylthio)phosphinyl-5'-O-methyl>-6-N-benzoyladenosine 3'-phosphorodianilidate

Base Information

Chemical Name:2'-O-bis(phenylthio)phosphinyl-5'-O-methyl>-6-N-benzoyladenosine 3'-phosphorodianilidate
CAS No.:97997-68-7
Molecular Formula:C₈₄H₅₄Cl₆N₁₀O₁₃P₂S₂
Molecular Weight:1750.21
Hs Code.:

2'-O-bis(phenylthio)phosphinyl-5'-O-<tris<4-(4,5-dichlorophthalimido)phenyl>methyl>-6-N-benzoyladenosine 3'-phosphorodianilidate

Synonyms:2'-O-bis(phenylthio)phosphinyl-5'-O-methyl>-6-N-benzoyladenosine 3'-phosphorodianilidate

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Chemical Property of 2'-O-bis(phenylthio)phosphinyl-5'-O-methyl>-6-N-benzoyladenosine 3'-phosphorodianilidate

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Technology Process of 2'-O-bis(phenylthio)phosphinyl-5'-O-methyl>-6-N-benzoyladenosine 3'-phosphorodianilidate

There total 1 articles about 2'-O-bis(phenylthio)phosphinyl-5'-O-methyl>-6-N-benzoyladenosine 3'-phosphorodianilidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 67941-87-1
cyclohexylammonium S,S-diphenyl phosphorodithioate

: 97997-67-6
5'-O-methyl>-6-N-benzoyladenosine 3'-phosphorodianilidate

: 97997-68-7
2'-O-bis(phenylthio)phosphinyl-5'-O-methyl>-6-N-benzoyladenosine 3'-phosphorodianilidate

Guidance literature:: With 1H-tetrazole; 2,4,6-trimethyl-1,3-benzenedisulfonyl dichloride; In pyridine; for 0.25h;
DOI:10.1246/bcsj.64.588

Reference yield:

: 97997-68-7
2'-O-bis(phenylthio)phosphinyl-5'-O-methyl>-6-N-benzoyladenosine 3'-phosphorodianilidate

: pyridinium phosphinate

: 97997-70-1
triethylammonium S-phenyl 3'-O-dianilinophosphinyl-5'-O-methyl>-6-N-benzoyladenosine 2'-phosphorothioate

Guidance literature:: In pyridine; for 1h; Yield given; Ambient temperature;
DOI:10.1021/ja00306a046

Reference yield:

: 15715-58-9
triethylamine carbonate

: 97997-68-7
2'-O-bis(phenylthio)phosphinyl-5'-O-methyl>-6-N-benzoyladenosine 3'-phosphorodianilidate

: triethylammonium 2'-O-bis(phenylthio)phosphinyl-5'-O-methyl>-6-N-benzoyladenosine 3'-phosphate

Guidance literature:: With pyridine; acetic anhydride; acetic acid; isopentyl nitrite; Yield given. Multistep reaction; 1) 11 h, 2) CH₂Cl₂;
DOI:10.1246/bcsj.64.588