N-((2R,3S)-tert-butyl-(tert-butyldimethylsilyloxy)-3-amino-4-hydroxybutan-2-ylcarbamoyl)-N'-(benzyloxycarbonyl)hydrazine carboxylic acid benzyl ester

Base Information

Chemical Name:N-((2R,3S)-tert-butyl-(tert-butyldimethylsilyloxy)-3-amino-4-hydroxybutan-2-ylcarbamoyl)-N'-(benzyloxycarbonyl)hydrazine carboxylic acid benzyl ester
CAS No.:1174341-30-0
Molecular Formula:C₃₁H₄₇N₃O₈Si
Molecular Weight:617.815
Hs Code.:

N-((2R,3S)-tert-butyl-(tert-butyldimethylsilyloxy)-3-amino-4-hydroxybutan-2-ylcarbamoyl)-N'-(benzyloxycarbonyl)hydrazine carboxylic acid benzyl ester

Synonyms:N-((2R,3S)-tert-butyl-(tert-butyldimethylsilyloxy)-3-amino-4-hydroxybutan-2-ylcarbamoyl)-N'-(benzyloxycarbonyl)hydrazine carboxylic acid benzyl ester

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Chemical Property of N-((2R,3S)-tert-butyl-(tert-butyldimethylsilyloxy)-3-amino-4-hydroxybutan-2-ylcarbamoyl)-N'-(benzyloxycarbonyl)hydrazine carboxylic acid benzyl ester

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Technology Process of N-((2R,3S)-tert-butyl-(tert-butyldimethylsilyloxy)-3-amino-4-hydroxybutan-2-ylcarbamoyl)-N'-(benzyloxycarbonyl)hydrazine carboxylic acid benzyl ester

There total 1 articles about N-((2R,3S)-tert-butyl-(tert-butyldimethylsilyloxy)-3-amino-4-hydroxybutan-2-ylcarbamoyl)-N'-(benzyloxycarbonyl)hydrazine carboxylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2449-05-0
dibenzyl azodicarboxylate

: 144751-63-3
tert-butyl ((tert-butyldimethylsilyl)oxy)carbamate

: 123-73-9,4170-30-3
crotonaldehyde

: 1174341-30-0
N-((2R,3S)-tert-butyl-(tert-butyldimethylsilyloxy)-3-amino-4-hydroxybutan-2-ylcarbamoyl)-N'-(benzyloxycarbonyl)hydrazine carboxylic acid benzyl ester

: N-(tert-butyl-(tert-butyldimethylsilyloxy)-3-amino-4-hydroxybutan-2-ylcarbamoyl)-N'-(benzyloxycarbonyl)hydrazine carboxylic acid benzyl ester

Guidance literature:: tert-butyl ((tert-butyldimethylsilyl)oxy)carbamate; crotonaldehyde; In chloroform; at -20 ℃; for 0.25h;

With (2S,5S)-5-benzyl-2-tert-butyl-3-methylimidazolidin-4-one trifluoromethanesulfonic acid salt; In chloroform; at -20 ℃; for 48h;

dibenzyl azodicarboxylate; optical yield given as %ee; Further stages;