(R)-(-)-1-methylheptyl 4'-[4-(3-hydroxypropyloxy)benzoyloxy]biphenyl-4-carboxylate

Base Information

Chemical Name:(R)-(-)-1-methylheptyl 4'-[4-(3-hydroxypropyloxy)benzoyloxy]biphenyl-4-carboxylate
CAS No.:902755-95-7
Molecular Formula:C₃₁H₃₆O₆
Molecular Weight:504.623
Hs Code.:

Synonyms:(R)-(-)-1-methylheptyl 4'-[4-(3-hydroxypropyloxy)benzoyloxy]biphenyl-4-carboxylate

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Chemical Property of (R)-(-)-1-methylheptyl 4'-[4-(3-hydroxypropyloxy)benzoyloxy]biphenyl-4-carboxylate

Chemical Property:

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Technology Process of (R)-(-)-1-methylheptyl 4'-[4-(3-hydroxypropyloxy)benzoyloxy]biphenyl-4-carboxylate

There total 5 articles about (R)-(-)-1-methylheptyl 4'-[4-(3-hydroxypropyloxy)benzoyloxy]biphenyl-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 46350-87-2
4-(3-hydroxypropyloxy)benzoic acid

: 121687-76-1
4'-hydroxy-biphenyl-4-carboxylic acid (R)-1-methyl-heptyl ester

: 902755-95-7
(R)-(-)-1-methylheptyl 4'-[4-(3-hydroxypropyloxy)benzoyloxy]biphenyl-4-carboxylate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 24h;
DOI:10.1039/b517913k

Reference yield:

: 3981-65-5
4-(3-hydroxypropoxy)-benzoic acid methyl ester

: 902755-95-7
(R)-(-)-1-methylheptyl 4'-[4-(3-hydroxypropyloxy)benzoyloxy]biphenyl-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 5.29 g / aq. KOH / ethanol / Heating

2: 96 percent / 4-(dimethylamino)pyridine; 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide*HCl / dimethylformamide / 24 h / 20 °C

With dmap; potassium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; N,N-dimethyl-formamide;
DOI:10.1039/b517913k

Reference yield:

: 6169-06-8,113301-48-7,4128-32-9
(S)-2-Octanol

: 902755-95-7
(R)-(-)-1-methylheptyl 4'-[4-(3-hydroxypropyloxy)benzoyloxy]biphenyl-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: diisopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran

2: 96 percent / 4-(dimethylamino)pyridine; 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide*HCl / dimethylformamide / 24 h / 20 °C

With dmap; di-isopropyl azodicarboxylate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/b517913k