1-(4,7-Dimethoxy-6-hydroxy-5-benzofuryl)-3-(4-methoxyphenyl)-propan-1,3-dion

Base Information

Chemical Name:1-(4,7-Dimethoxy-6-hydroxy-5-benzofuryl)-3-(4-methoxyphenyl)-propan-1,3-dion
CAS No.:85518-05-4
Molecular Formula:C₂₀H₁₈O₇
Molecular Weight:370.359
Hs Code.:

Synonyms:1-(4,7-Dimethoxy-6-hydroxy-5-benzofuryl)-3-(4-methoxyphenyl)-propan-1,3-dion

Suppliers and Price of 1-(4,7-Dimethoxy-6-hydroxy-5-benzofuryl)-3-(4-methoxyphenyl)-propan-1,3-dion

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1-(4,7-Dimethoxy-6-hydroxy-5-benzofuryl)-3-(4-methoxyphenyl)-propan-1,3-dion

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1-(4,7-Dimethoxy-6-hydroxy-5-benzofuryl)-3-(4-methoxyphenyl)-propan-1,3-dion

There total 10 articles about 1-(4,7-Dimethoxy-6-hydroxy-5-benzofuryl)-3-(4-methoxyphenyl)-propan-1,3-dion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 85518-00-9
(5-Acetyl-4,7-dimethoxy-6-benzofuranyl)-4-methoxybenzoat

: 85518-05-4
1-(4,7-Dimethoxy-6-hydroxy-5-benzofuryl)-3-(4-methoxyphenyl)-propan-1,3-dion

Guidance literature:: With potassium hydroxide; In pyridine; at 80 ℃; for 0.25h;
DOI:10.1002/ardp.19833160304

Reference yield:

: 484-51-5
5-acetyl-6-hydroxy-4,7-dimethoxybenzofuran

: 85518-05-4
1-(4,7-Dimethoxy-6-hydroxy-5-benzofuryl)-3-(4-methoxyphenyl)-propan-1,3-dion

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / pyridine / CHCl₃ / 0.5 h / 50 °C

2: 84 percent / KOH / pyridine / 0.25 h / 80 °C

With pyridine; potassium hydroxide; In pyridine; chloroform;
DOI:10.1002/ardp.19833160304

Reference yield:

: 52249-80-6
2,4-dihydroxy-3,6-dimethoxybenzaldehyde

: 85518-05-4
1-(4,7-Dimethoxy-6-hydroxy-5-benzofuryl)-3-(4-methoxyphenyl)-propan-1,3-dion

Guidance literature:: Multi-step reaction with 8 steps

1: K₂CO₃; acetone

2: K₂CO₃; acetone

3: sodium ethylate

4: palladium/charcoal; acetic acid / Hydrogenation

5: nitrobenzene; aluminium chloride / Behandeln des Reaktionsprodukts mit wss. Natronlauge

6: quinoline; copper-powder

7: pyridine

8: sodium amide; toluene

With pyridine; quinoline; palladium on activated charcoal; aluminium trichloride; sodium ethanolate; copper; potassium carbonate; sodium amide; acetic acid; nitrobenzene; acetone; toluene;
DOI:10.1039/jr9490000302