C₁₉H₁₃F₃N₄O₂

Base Information

Chemical Name:C₁₉H₁₃F₃N₄O₂
CAS No.:1620328-33-7
Molecular Formula:C₁₉H₁₃F₃N₄O₂
Molecular Weight:386.333
Hs Code.:

C<sub>19</sub>H<sub>13</sub>F<sub>3</sub>N<sub>4</sub>O<sub>2</sub>

Synonyms:C₁₉H₁₃F₃N₄O₂

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Chemical Property of C₁₉H₁₃F₃N₄O₂

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Technology Process of C₁₉H₁₃F₃N₄O₂

There total 14 articles about C₁₉H₁₃F₃N₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1160501-79-0
C₁₉H₁₅F₃N₄O

: 1620328-33-7
C₁₉H₁₃F₃N₄O₂

Guidance literature:: With 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium bromide; In water; acetone; at 0 ℃; for 0.333333h;
DOI:10.1016/j.bmcl.2014.05.082

Reference yield:

: 1620328-25-7
C₄₀H₃₁F₃N₄O₂

: 1620328-33-7
C₁₉H₁₃F₃N₄O₂

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / tetrahydrofuran; methanol / 1 h / 0 °C

2: N-tris(hydroxymethyl)methyl-2-aminoethanesulfonic acid; trifluoroacetic acid / dichloromethane / 2 h / 0 °C

3: sodium hypochlorite; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium bromide / water; acetone / 0.33 h / 0 °C

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; N-tris(hydroxymethyl)methyl-2-aminoethanesulfonic acid; trifluoroacetic acid; sodium bromide; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; acetone;
DOI:10.1016/j.bmcl.2014.05.082

Reference yield:

: 1620328-45-1
C₃₈H₂₉F₃N₄O

: 1620328-33-7
C₁₉H₁₃F₃N₄O₂

Guidance literature:: Multi-step reaction with 2 steps

1: N-tris(hydroxymethyl)methyl-2-aminoethanesulfonic acid; trifluoroacetic acid / dichloromethane / 2 h / 0 °C

2: sodium hypochlorite; 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium bromide / water; acetone / 0.33 h / 0 °C

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; N-tris(hydroxymethyl)methyl-2-aminoethanesulfonic acid; trifluoroacetic acid; sodium bromide; In dichloromethane; water; acetone;
DOI:10.1016/j.bmcl.2014.05.082