ethyl N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)carbamate

Base Information

Chemical Name:ethyl N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)carbamate
CAS No.:82082-31-3
Molecular Formula:C₂₃H₁₈Cl₃NO₃
Molecular Weight:462.76
Hs Code.:

Synonyms:ethyl N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)carbamate

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Chemical Property of ethyl N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)carbamate

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Technology Process of ethyl N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)carbamate

There total 6 articles about ethyl N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6628-86-0
5-chloro-2-nitrobenzaldehyde

: 82082-31-3
ethyl N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)carbamate

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) n-BuLi / 1.) THF, -78 deg C, 20 min, 2.) THF, -78 deg C, 1 h

2: Jones reagent, acetic acid / diethyl ether / 12 h / Ambient temperature

3: 62 percent / H₂ / Raney nickel / ethanol / 8 h / 760 Torr

4: 84 percent / pyridine / diethyl ether; CH₂Cl₂ / 1 h / Ambient temperature

5: 1.) n-BuLi / 1.) hexane, DMSO, 2.) hexane, DMSO, RT, 1 h

With pyridine; n-butyllithium; jones reagent; hydrogen; acetic acid; nickel; In diethyl ether; ethanol; dichloromethane;
DOI:10.1021/jm00351a009

Reference yield:

: 82082-25-5
(2,6-dichlorophenyl)(5-chloro-2-nitrophenyl)methanone

: 82082-31-3
ethyl N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / H₂ / Raney nickel / ethanol / 8 h / 760 Torr

2: 84 percent / pyridine / diethyl ether; CH₂Cl₂ / 1 h / Ambient temperature

3: 1.) n-BuLi / 1.) hexane, DMSO, 2.) hexane, DMSO, RT, 1 h

With pyridine; n-butyllithium; hydrogen; nickel; In diethyl ether; ethanol; dichloromethane;
DOI:10.1021/jm00351a009

Reference yield:

: 875644-89-6
(2-nitro-5-chlorophenyl)(2,6-dichlorophenyl)methanol

: 82082-31-3
ethyl N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-(phenylmethyl)carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: Jones reagent, acetic acid / diethyl ether / 12 h / Ambient temperature

2: 62 percent / H₂ / Raney nickel / ethanol / 8 h / 760 Torr

3: 84 percent / pyridine / diethyl ether; CH₂Cl₂ / 1 h / Ambient temperature

4: 1.) n-BuLi / 1.) hexane, DMSO, 2.) hexane, DMSO, RT, 1 h

With pyridine; n-butyllithium; jones reagent; hydrogen; acetic acid; nickel; In diethyl ether; ethanol; dichloromethane;
DOI:10.1021/jm00351a009