(3E,8E,10E)-10-methyl-13-phenyl-6,6-(dicarboethoxy)-1,3,8,10-tridecatetraene

Base Information

Chemical Name:(3E,8E,10E)-10-methyl-13-phenyl-6,6-(dicarboethoxy)-1,3,8,10-tridecatetraene
CAS No.:190667-53-9
Molecular Formula:C₂₆H₃₄O₄
Molecular Weight:410.554
Hs Code.:

Synonyms:(3E,8E,10E)-10-methyl-13-phenyl-6,6-(dicarboethoxy)-1,3,8,10-tridecatetraene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3E,8E,10E)-10-methyl-13-phenyl-6,6-(dicarboethoxy)-1,3,8,10-tridecatetraene

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Technology Process of (3E,8E,10E)-10-methyl-13-phenyl-6,6-(dicarboethoxy)-1,3,8,10-tridecatetraene

There total 3 articles about (3E,8E,10E)-10-methyl-13-phenyl-6,6-(dicarboethoxy)-1,3,8,10-tridecatetraene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 70925-46-1,56161-69-4
(2E)-2-methyl-5-phenyl-2-pentenal

: 190667-51-7
(4E)-4-methyl-7-phenyl-1,4-heptadien-3-ol acetate

: 190667-53-9
(3E,8E,10E)-10-methyl-13-phenyl-6,6-(dicarboethoxy)-1,3,8,10-tridecatetraene

Guidance literature:: With tributylphosphine; sodium hydride; palladium diacetate; In tetrahydrofuran; for 8h; Heating;
DOI:10.1021/ja962748g

Reference yield:

: 70925-46-1,56161-69-4
(2E)-2-methyl-5-phenyl-2-pentenal

: 190667-53-9
(3E,8E,10E)-10-methyl-13-phenyl-6,6-(dicarboethoxy)-1,3,8,10-tridecatetraene

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / tetrahydrofuran / 8 h / 20 °C

2: 89 percent / DMAP; Et₃N / 8 h / 0 °C

3: 75 percent / NaH; Bu₃P / Pd(OAc)2 / tetrahydrofuran / 8 h / Heating

With dmap; tributylphosphine; sodium hydride; triethylamine; palladium diacetate; In tetrahydrofuran; 1: Grignard reaction / 2: Acetylation / 3: Substitution;
DOI:10.1021/ja962748g

Reference yield:

: 190667-49-3
(4E)-4-methyl-7-phenyl-1,4-heptadien-3-ol

: 190667-53-9
(3E,8E,10E)-10-methyl-13-phenyl-6,6-(dicarboethoxy)-1,3,8,10-tridecatetraene

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / DMAP; Et₃N / 8 h / 0 °C

2: 75 percent / NaH; Bu₃P / Pd(OAc)2 / tetrahydrofuran / 8 h / Heating

With dmap; tributylphosphine; sodium hydride; triethylamine; palladium diacetate; In tetrahydrofuran; 1: Acetylation / 2: Substitution;
DOI:10.1021/ja962748g