N-(phenylsulfonyl)-2-methylenepiperidine

Base Information

Chemical Name:N-(phenylsulfonyl)-2-methylenepiperidine
CAS No.:97462-73-2
Molecular Formula:C₁₂H₁₅NO₂S
Molecular Weight:237.323
Hs Code.:

Synonyms:N-(phenylsulfonyl)-2-methylenepiperidine

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Chemical Property of N-(phenylsulfonyl)-2-methylenepiperidine

Chemical Property:

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Technology Process of N-(phenylsulfonyl)-2-methylenepiperidine

There total 5 articles about N-(phenylsulfonyl)-2-methylenepiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 25630-24-4
N,N-diallylbenzenesulfonamide

: 97462-72-1
N-(phenylsulfonyl)-3-methyl-4-methylenepyrrolidine

: 97462-73-2
N-(phenylsulfonyl)-2-methylenepiperidine

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; 1,5-cis,cis-cyclooctadiene; [1,3-bis(2,4,6-trimethylphenyl)imidazol]-2-ylidene; sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate; allyl bromide; In dichloromethane; at 0 - 23 ℃; for 5h;
DOI:10.1002/adsc.201400237

Reference yield:

: 50487-70-2
N-allylbenzenesulfonamide

: 97462-73-2
N-(phenylsulfonyl)-2-methylenepiperidine

Guidance literature:: Multi-step reaction with 2 steps

2: Bu₃SnH / add of PhSeSePh; var. conc.

With tri-n-butyl-tin hydride;
DOI:10.1016/0040-4039(96)00526-6

Reference yield:

: 98-10-2
benzenesulfonamide

: 97462-73-2
N-(phenylsulfonyl)-2-methylenepiperidine

Guidance literature:: Multi-step reaction with 3 steps

1: 30 percent / K₂CO₃ / acetone / 36 h / Heating

2: 76 percent / cesium fluoride / dimethylformamide / 36 h / Ambient temperature

3: 300 mg / tri-n-butyltin hydride, 2,2'-azobisisobutyronitrile (AIBN) / benzene / 8 h / Heating

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; potassium carbonate; cesium fluoride; In N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1021/jo00350a038