cis,exo-2,3-norbornane-fused 5-methyl-2,3-dihydrobenzothiophene 1,1-dioxide

Base Information

• Chemical Name: cis,exo-2,3-norbornane-fused 5-methyl-2,3-dihydrobenzothiophene 1,1-dioxide
• CAS No.: 132560-64-6
• Molecular Formula: C₁₄H₁₆O₂S
• Molecular Weight: 248.346

Synonyms:cis,exo-2,3-norbornane-fused 5-methyl-2,3-dihydrobenzothiophene 1,1-dioxide

Chemical Property of cis,exo-2,3-norbornane-fused 5-methyl-2,3-dihydrobenzothiophene 1,1-dioxide

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Technology Process of cis,exo-2,3-norbornane-fused 5-methyl-2,3-dihydrobenzothiophene 1,1-dioxide

There total 5 articles about cis,exo-2,3-norbornane-fused 5-methyl-2,3-dihydrobenzothiophene 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

norborn-2-ene (498-66-8) + p-tolylazoxy p-tolyl sulphone (60126-95-6) → 4-Methylbiphenyl (644-08-6) + cis,exo-2,3-norbornane-fused 5-methyl-2,3-dihydrobenzothiophene 1,1-dioxide (132560-64-6)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In benzene; at 80 ℃; for 24h;

Reference yield: 70.0%

norborn-2-ene (498-66-8) + phenylazoxy p-tolyl sulphone (60126-94-5) → biphenyl (92-52-4,1594-86-1) + cis,exo-2,3-norbornane-fused 5-methyl-2,3-dihydrobenzothiophene 1,1-dioxide (132560-64-6)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In benzene; at 80 ℃; for 24h;

Reference yield: 53.0%

norborn-2-ene (498-66-8) + (4-methylphenyl)azo 4-methylphenyl sulfone (33604-67-0) → 4-Methylbiphenyl (644-08-6) + cis,exo-2,3-norbornane-fused 5-methyl-2,3-dihydrobenzothiophene 1,1-dioxide (132560-64-6)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In benzene; at 80 ℃; for 24h;

upstream raw materials:

norborn-2-ene

p-tolylazoxy p-tolyl sulphone

(4-methylphenyl)azo 4-methylphenyl sulfone

phenylazoxy p-tolyl sulphone

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