C₄₉H₆₄N₂O₂₈

Base Information

Chemical Name:C₄₉H₆₄N₂O₂₈
CAS No.:552831-63-7
Molecular Formula:C₄₉H₆₄N₂O₂₈
Molecular Weight:1129.04
Hs Code.:

C<sub>49</sub>H<sub>64</sub>N<sub>2</sub>O<sub>28</sub>

Synonyms:C₄₉H₆₄N₂O₂₈

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Chemical Property of C₄₉H₆₄N₂O₂₈

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Technology Process of C₄₉H₆₄N₂O₂₈

There total 7 articles about C₄₉H₆₄N₂O₂₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 402948-43-0
methyl (phenyl 4,7,8,9-tetra-O-acetyl-3,5-dideoxy-2-thio-5-(2,2,2-trichloroethoxycarbonylamino)-D-glycero-β-D-galacto-2-nonulopyranosid)onate

: 552831-63-7
C₄₉H₆₄N₂O₂₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: 66 percent / molecular sieves 4 Angstroem; NIS; TfOH / acetonitrile / 1 h / -25 °C

2.1: Zn; glacial AcOH / 1.5 h / 20 °C

2.2: 54 percent / NaHCO₃; HOBt; EDC / acetonitrile / 20 °C

3.1: Zn; glacial AcOH / 1.5 h / 20 °C

4.1: 0.136 g / iPr₂NEt / CH₂Cl₂ / 2 h / 0 °C

With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; acetic acid; N-ethyl-N,N-diisopropylamine; zinc; In dichloromethane; acetonitrile;
DOI:10.1002/chem.200390101

Reference yield:

: 552831-43-3
(2R,4S,5R,6R)-4-Acetoxy-2-benzyloxycarbonylmethoxy-6-((1S,2R)-1,2,3-triacetoxy-propyl)-5-(2,2,2-trichloro-ethoxycarbonylamino)-tetrahydro-pyran-2-carboxylic acid methyl ester

: 552831-63-7
C₄₉H₆₄N₂O₂₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: 100 percent / H₂ / 10percent Pd/C / ethyl acetate

2.1: Zn; glacial AcOH / 1.5 h / 20 °C

2.2: 54 percent / NaHCO₃; HOBt; EDC / acetonitrile / 20 °C

3.1: Zn; glacial AcOH / 1.5 h / 20 °C

4.1: 0.136 g / iPr₂NEt / CH₂Cl₂ / 2 h / 0 °C

With hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; zinc; 10percent Pd/C; In dichloromethane; ethyl acetate;
DOI:10.1002/chem.200390101